Cotton rose leaf extractive and preparation method thereof, anti-corrosion composition and preparation method thereof and cosmetic composition
A technology of Hibiscus hibiscus leaves and extracts, which is applied in cosmetics, cosmetic preparations, cosmetic preparations and other directions, can solve the problems of reducing the viscosity of cosmetic systems, low extraction efficiency, affecting stability, etc., and achieves the promotion of dissolution, high extraction rate, High stability effect
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[0052] According to a first aspect of the present invention, there is provided a method for preparing hibiscus leaf extract, comprising the following steps:
[0053] S1. Hibiscus leaf powder is provided, and the mixed solution of hibiscus leaf powder and solvent is subjected to low-temperature and high-pressure homogenization;
[0054] S2. Concentrating the filtrate obtained after ultrasonic extraction of the mixture obtained by the low temperature and high pressure homogeneous treatment to obtain a concentrated suspension;
[0055] S3. purifying the concentrated suspension through a polyamide resin to obtain an eluate;
[0056] S4. Decolorizing and separating the eluent to obtain hibiscus leaf extract.
[0057] Specifically, hibiscus leaves are the leaves of Hibiscus hibiscus in Malvaceae, which is a traditional Chinese medicine, and its main components are flavonoids and sterols.
[0058] Hibiscus leaf powder is usually a powdery product obtained by crushing hibiscus leave...
Embodiment approach
[0123] As a preferred embodiment of the present invention, the antiseptic composition comprises the following raw materials in mass fraction: 2-8% of hibiscus leaf extract, 30-60% of polyol, 5-15% of solubilizer, and water to make up the remaining quantity;
[0124] Preferably, the antiseptic composition is made of the following raw materials in mass fraction: Hibiscus hibiscus leaf extract 2.5-8%, polyol 35-55%, solubilizer 5-13%, and water to make up the balance.
[0125] By further limiting the dosage of each raw material of the antiseptic composition, the antiseptic, antibacterial and anti-oxidation effects of the antiseptic composition are more significant, and at the same time, the irritation to the skin is smaller, and the safety is further improved.
[0126] As a preferred embodiment of the present invention, the polyhydric alcohol includes one or a combination of at least two of ethylhexylglycerin, caprylyl glycol, 1,2-pentanediol or 1,2-hexanediol.
[0127] Ethylhex...
Embodiment 1
[0146] The present embodiment provides a kind of preparation method of hibiscus leaf extract, comprising the following steps:
[0147] (1) removing impurities from the dried hibiscus leaves, and pulverizing them with a plant pulverizer, and crossing a 50-mesh stainless steel mesh sieve to obtain hibiscus leaf powder;
[0148] Add hibiscus leaves to 80% ethanol aqueous solution, pretreat it with a low temperature and high pressure homogenizer, the homogenization temperature is 4°C, the homogenization pressure is 5.5MPa, and the homogenization time is 30s;
[0149] (2) Extract the mixture obtained by homogeneous treatment at low temperature and high pressure using ultrasonic-assisted extraction method, ultrasonic power 304W, solid-liquid ratio 1:30, extraction temperature 35°C, extraction time 0.5h, after extraction, suction filter, and collect the filtrate;
[0150] The obtained filtrate was concentrated under reduced pressure to 1 / 6 of the original volume to obtain a concentra...
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