Processing technology of high-performance antibacterial polypropylene spun-bonded non-woven fabric
A technology of polypropylene spunbonding and processing technology, which is applied in non-woven fabrics, textiles, papermaking, biochemical fiber treatment, etc. It can solve the problems of high cost, weak antibacterial ability, and human injury of chemical agents, and achieves stable antibacterial performance and antibacterial timeliness Long-lasting, pronounced antimicrobial properties
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Embodiment 1
[0027] (1) Preparation of carboxylated polypropylene: fully mix 15g polypropylene powder and 5g nitric acid with a mass fraction of 70%, and then heat to 130°C for heat preservation and stirring reaction. After the reaction, the resulting mixture is naturally cooled to room temperature, and washed to remove nitric acid, and finally vacuum-dried and pulverized into powder to obtain carboxylated polypropylene;
[0028] (2) Antibacterial modification of polypropylene: dissolve 5g of chitosan hydrochloride in water, then add 35g of the prepared carboxylated polypropylene, stir well, and add dilute sulfuric acid dropwise to adjust the pH to 5, then heat to reflux Insulate and stir the reaction. After the reaction, cool the resulting mixture to room temperature naturally, then add dropwise sodium carbonate solution to adjust the pH value to 7, filter, wash with water to remove salt, and finally vacuum-dry and pulverize to make granules to obtain modified chitosan. polypropylene;
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Embodiment 2
[0032] (1) Preparation of carboxylated polypropylene: fully mix 20g of polypropylene powder and 5g of nitric acid with a mass fraction of 70%, and then heat to 130°C for heat preservation and stirring reaction. After the reaction, the resulting mixture is naturally cooled to room temperature, and washed to remove nitric acid, and finally vacuum-dried and pulverized into powder to obtain carboxylated polypropylene;
[0033] (2) Antibacterial modification of polypropylene: Dissolve 8g of chitosan hydrochloride in water, then add 50g of the prepared carboxylated polypropylene, stir well, and add dilute sulfuric acid dropwise to adjust the pH value to 5, then heat to reflux state Insulate and stir the reaction. After the reaction, cool the resulting mixture to room temperature naturally, then add dropwise sodium carbonate solution to adjust the pH value to 7, filter, wash with water to remove salt, and finally vacuum-dry and pulverize to make granules to obtain modified chitosan. ...
Embodiment 3
[0037] (1) Preparation of carboxylated polypropylene: fully mix 20g of polypropylene powder and 5g of nitric acid with a mass fraction of 70%, and then heat to 130°C for heat preservation and stirring reaction. After the reaction, the resulting mixture is naturally cooled to room temperature, and washed to remove nitric acid, and finally vacuum-dried and pulverized into powder to obtain carboxylated polypropylene;
[0038] (2) Antibacterial modification of polypropylene: Dissolve 8g of chitosan hydrochloride in water, then add 50g of the prepared carboxylated polypropylene, stir well, and add dilute sulfuric acid dropwise to adjust the pH value to 5, then heat to reflux state Insulate and stir the reaction. After the reaction, cool the resulting mixture to room temperature naturally, then add dropwise sodium carbonate solution to adjust the pH value to 7, filter, wash with water to remove salt, and finally vacuum-dry and pulverize to make granules to obtain modified chitosan. ...
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