Preparation method of high-strength porous sound absorbing material
A porous sound-absorbing, high-strength technology, applied in glass manufacturing equipment, manufacturing tools, glass molding, etc., can solve the problem of low utilization of blast furnace slag, achieve no secondary pollution, good comprehensive performance, and reduce accumulation Effect
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Embodiment 1
[0021] Add 40.5wt.% high-titanium blast furnace slow cooling slag, 50.5wt.% waste glass powder, 1wt.% AlN, 5wt.% borax. Ball mill and mix at a speed of 180r / min for 30min in a ball mill. Put it into a corundum crucible and send it to a resistance furnace for sintering. First, the temperature is raised to 400°C at a rate of 8°C / min and kept at a temperature of 20 minutes, and then raised to 1020°C at a rate of 10°C / min and kept at a temperature of 60 minutes for sintering. After sintering, cool down to 500°C at a rate of 25°C / s, and finally cool slowly to room temperature at a rate of 5°C / s to prepare a high-strength porous sound-absorbing material.
[0022] The volume density of the high-strength porous sound-absorbing material is 0.95g / cm 3 , The opening rate is 50.43%, the average pore diameter is 1.28mm, the compressive strength is 12.49MPa, and the average sound absorption coefficient is 0.29.
Embodiment 2
[0024] Add 39wt.% high-titanium blast furnace slow cooling slag, 52wt.% waste glass powder, 2wt.% AlN, 7wt.% borax. Ball mill and mix at a speed of 250r / min for 25min in a ball mill. Put it into a corundum crucible and send it to a resistance furnace for sintering. First, the temperature is raised to 400°C at a rate of 5°C / min and kept at a temperature of 20 minutes, and then raised to 1000°C at a rate of 10°C / min and kept at a temperature of 40 minutes for sintering. After sintering, cool to 500°C at a rate of 30°C / s, and finally cool slowly to room temperature at a rate of 4°C / s to prepare a high-strength porous sound-absorbing material.
[0025] The volume density of the high-strength porous sound-absorbing material is 0.96g / cm 3 , The opening rate is 53.62%, the average pore diameter is 0.88mm, the compressive strength is 16.64MPa, and the average sound absorption coefficient is 0.36.
Embodiment 3
[0027] Add 48wt.% high-titanium blast furnace slow cooling slag, 42wt.% waste glass powder, 4wt.% AlN, 6wt.% borax. Ball mill and mix at a speed of 300r / min for 30min in a ball mill. Put it into a corundum crucible and send it to a resistance furnace for sintering. First, the temperature is raised to 400°C at a rate of 8°C / min and kept at a temperature of 20 minutes, and then raised to 1020°C at a rate of 10°C / min and kept at a temperature of 60 minutes for sintering. After sintering, cool to 500°C at a rate of 28°C / s, and finally cool slowly to room temperature at a rate of 5°C / s to prepare a high-strength porous sound-absorbing material.
[0028] The volume density of the high-strength porous sound-absorbing material is 1.17g / cm 3 , The opening rate is 55.34%, the average pore diameter is 0.70mm, the compressive strength is 15.65MPa, and the average sound absorption coefficient is 0.39.
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