Nano antibacterial material preparation method
A technology of nanometer antibacterial materials and inorganic nanomaterials, which is applied in the field of preparation of nanometer antibacterial materials, can solve the problems such as the reduction of material hardness, toughness and tear strength, the influence of long-term use performance of materials, and the inability to maintain for a long time, so as to achieve excellent antibacterial properties, The effect of broad market use value and long service life
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Embodiment 1
[0026] A preparation method of nano antibacterial material, comprising the following preparation steps:
[0027] a. Mix polyester polyol and polyether polyol into the reaction kettle, heat and stir at 150°C, then lower the temperature to 50°C after 10 minutes, and perform dehydration treatment for 40 minutes to obtain material 1;
[0028] b. Add anti-blocking agent, organic antibacterial agent and inorganic antibacterial agent to material 1 and mix evenly, vacuumize to -0.1MPa under heating at 90°C, then cool down to 75°C for dehydration for 2 hours, then import it into the internal mixer and add Catalyst, carry out banburying reaction 4h, obtain material two;
[0029] c. Mix the nano-silver-zinc composite material, surfactant and deionized water into a mixer, grind and stir for 5 hours, then add inorganic nano-materials and inorganic fillers and stir evenly to obtain material 3;
[0030] d. Mix material 2 and material 3, add isocyanate, chain extender and lubricant, stir at ...
Embodiment 2
[0041] A preparation method of nano antibacterial material, comprising the following preparation steps:
[0042] a. Mix polyester polyol and polyether polyol into the reaction kettle, heat and stir at 120°C, lower the temperature to 40°C after 10 minutes, perform dehydration treatment for 40 minutes, and obtain material 1;
[0043] b. Add anti-blocking agent, organic antibacterial agent and inorganic antibacterial agent to material 1 and mix evenly, vacuumize to -0.1MPa under heating at 90°C, then cool down to 65°C for dehydration for 1 hour, then import it into the internal mixer and add Catalyst, carry out banburying reaction 4h, obtain material two;
[0044] c. Mix the nano-silver-zinc composite material, surfactant and deionized water into a mixer, grind and stir for 3 hours, then add inorganic nano-materials and inorganic fillers and stir evenly to obtain material 3;
[0045] d. Mix material 2 and material 3, add isocyanate, chain extender and lubricant, stir at 80°C for...
Embodiment 3
[0056] A preparation method of nano antibacterial material, comprising the following preparation steps:
[0057] a. Mix polyester polyol and polyether polyol into the reaction kettle, heat and stir at 150°C, lower the temperature to 50°C after 15 minutes, and perform dehydration treatment for 50 minutes to obtain material 1;
[0058] b. Add anti-blocking agent, organic antibacterial agent and inorganic antibacterial agent to material 1 and mix evenly, vacuumize to -0.1MPa under heating at 95°C, then cool down to 75°C for dehydration for 2 hours, then import it into the internal mixer and add Catalyst, carry out Banbury reaction 6h, obtain material two;
[0059] c. Mix the nano-silver-zinc composite material, surfactant and deionized water into a mixer, grind and stir for 5 hours, then add inorganic nano-materials and inorganic fillers and stir evenly to obtain material 3;
[0060] d. Mix material 2 and material 3, add isocyanate, chain extender and lubricant, stir at 90°C for...
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