Grease for elevator rope, elevator rope, and traction elevator
A technology for lubricating grease and slings, applied in lubricating compositions, textile cables, transportation and packaging, etc., can solve problems such as increased wear, increased pressure, and reduced tensile strength of slings, and achieves the effect of high wear resistance
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[0126] Hereinafter, although an Example and a comparative example are used and this invention is demonstrated concretely, this invention is not limited to these Examples.
[0127] (1) Evaluation method of sling oil and grease
[0128] (1-1) Determination of kinematic viscosity, consistency and dropping point of sling oil
[0129] The kinematic viscosity (40 degreeC, 100 degreeC) of a sling oil was measured based on JIS standard (JIS K2283). In addition, the consistency (unmixed consistency, mixed consistency) and dropping point of the grease were measured based on JIS standards (JIS K2220). In addition, the viscosity grade was evaluated based on ISO (International Organization for Standardization, International Organization for Standardization) 3448 from the value of the kinematic viscosity at 40°C of the sling oil.
[0130](1-2) Determination of traction coefficient
[0131] The traction coefficient was measured using a Ball on Disk (ball on disk) test device. This test d...
reference example 7
[0183] (2-10) Reference Example 7: Synthesis of Synthetic Oil 11
[0184] 1kg of terpinolene, 200mL of cyclohexane, 100ml of 1,2-diethoxyethane, and 100g of cation exchange resin as a catalyst were added to a 10L glass reaction vessel, heated at 60°C for 6 hours, and stirred. After the reaction, it was cooled in a 20° C. water bath, and the solid catalyst was filtered off. Use a rotary evaporator to recover the solvent and unreacted raw materials, add 500g of the reaction solution to a 1L autoclave, add 50g of nickel catalyst for hydrogenation, and seal it with a hydrogen pressure of 50kg / cm 2 (G), carry out hydrogenation at 120° C. for 4 hours, cool naturally to room temperature, and filter out the catalyst.
[0185] The obtained product was analyzed by gel filtration chromatography, and a dimer component (synthetic oil 11) was formed. The entire reaction solution was distilled under reduced pressure, and only the dimer component was fractionated.
[0186] (2-11) Reference...
Embodiment 1
[0191] In Examples 17 to 26, the synthetic oil in Example 1 was changed to other polycyclic naphthene compounds (synthetic oils 6 to 15). Table 4 shows the composition and evaluation results of the base oil. All showed high traction coefficient and wear resistance similarly to Example 1.
[0192] [Table 4]
[0193]
[0194] (2-14) Reference Example 9: Preparation of Thickener
[0195] In a 3 L glass reaction vessel, 30 g of ethylenediamine and 300 g of 12-hydroxystearic acid were dissolved in m-xylene, 15 g of iron(III) chloride hexahydrate was added as a catalyst, and the mixture was heated to reflux for 10 hours. After the product was filtered off, the product was isolated and purified by recrystallization.
[0196] The resulting product was analyzed by gel filtration chromatography, whereby fatty acid diamide (N,N'-ethylene-bis-12-hydroxystearamide) was obtained.
[0197] (2-15) Preparation and evaluation of the greases of Examples 27 to 33 and Comparative Example 2 ...
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