Agricultural environment-friendly antibacterial agent and preparation method thereof
An antibacterial agent and environmental protection technology, applied in the field of agricultural environmental protection antibacterial agent and its preparation, can solve the problems of human health threats, infiltration into crops, soil and water bodies, pollution of the environment, etc., achieve good efficacy, strengthen wetting penetration Function, the effect of easy availability of raw materials
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[0015] The present invention will be further described below in conjunction with specific embodiments.
[0016] A kind of preparation method (synthetic mechanism of agricultural environment-friendly antibacterial agent, see figure 1 ), including the following steps.
[0017] Step 1, eugenol acetate group modification: take 2g eugenol, 1g paraformaldehyde and dissolve in 100ml absolute ethanol, adjust PH=3 with HCl, heat up to 70°C, add 2.5g anhydrous zinc chloride, stir ( 300r / min) after 3h, add 3g of formic acid and 1.4g of aluminum trichloride, continue to react for 3h. The reaction solution was extracted 5 times with ether, and the organic phases were combined, dried with 6 g of anhydrous sodium sulfate, filtered, spin-dried with ether, and vacuum-dried at 90° C. for 10 h to obtain the target product, ie, acetoxyeugenol.
[0018] Step 2: Grafting monosaccharides to acetate eugenol: at 85°C, dissolve 6.4g acetate eugenol and 7.2g glucose in 280ml water, add them to a 500ml...
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