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A quality detection method for Zishen Ningshen Pills

A quality inspection method and a kidney-nourishing technology, applied in the field of medicine, can solve the problems of poor durability, long time consumption, and complicated operation, and achieve the effect of ensuring stability, controllability, and strong specificity.

Active Publication Date: 2020-05-12
GUANGDONG YIHETANG PHARMA CO LTD
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Problems solved by technology

In addition, in the analysis method, ultrasonic extraction is used to prepare the test solution twice, each time for 30 minutes, and then filtered, and the filtrates are combined and then constant volume. There are problems such as long extraction time, cumbersome operation, and the test substance is easy to remain on the filter paper.
[0004] Literature "HPLC method measures the content of paeoniflorin in Zishen Ningshen Pills" (Chinese medicinal materials: the 6th issue in 2002) adopts HPLC to measure the content of paeoniflorin in Zishen Ningshen Pills, dilute ethanol is used in the preparation of test solution Extract the solvent, centrifuge after ultrasonic extraction, and accurately absorb the supernatant to make up the volume. This method has the disadvantages of cumbersome operation and long time-consuming
No durability test was conducted, suggesting that the analytical method is limited to specific conditions, and the tolerance level of the measurement results is not known, indicating that its durability is not strong, and the reliability of the analytical method cannot be guaranteed

Method used

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  • A quality detection method for Zishen Ningshen Pills
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  • A quality detection method for Zishen Ningshen Pills

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Embodiment 1

[0036] A quality detection method for Zishen Ningshen Pill, characterized in that it comprises qualitative identification by thin-layer chromatography and content detection of Schisandrin A:

[0037] (1) Qualitative identification of dodder by thin layer chromatography:

[0038]Take 8g of this product, grind it finely, add 50ml of ethanol, sonicate for 30 minutes, filter, evaporate the filtrate to dryness, add 20ml of water to the residue to dissolve, extract with ether for 3 times, 20ml each time, discard the ether solution, and use ethyl acetate for the aqueous solution Extract 3 times, 20 ml each time, combine the ethyl acetate extracts, evaporate to dryness, add 1 ml of ethanol to the residue to dissolve, and use it as the test solution; take 1 g of the reference medicinal material of Dodder, add 50 ml of ethanol, sonicate for 30 minutes, filter, and evaporate the filtrate. Dry, add 20 ml of water to the residue to dissolve, from “extracted with ether for 3 times”, prepare...

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Abstract

The invention discloses a quality detection method of kidney-nourishing and nerve-calming pills. The quality detection method comprises thin-layer chromatographic qualitative identification and content detection of schizandrin. According to the quality detection method of the kidney-nourishing and nerve-calming pills, the thin-layer chromatographic qualitative identification for prepared polygonummultiflorum and semen cuscutae in the kidney-nourishing and nerve-calming pills is firstly built, and the content measurement is performed on the schizandrin. The detection method is relatively highin specificity and durability, and the accuracy, the repetitiveness and the stability of the detection method all can meet scientific research and production requirements, so that the stability and the controllability of product quality can be effectively guaranteed.

Description

technical field [0001] The invention belongs to the technical field of medicine, and particularly relates to a quality detection method for Zishen Ningshen Pills. Background technique [0002] Zishen Ningshen Pills is made from Rehmannia glutinosa, Chinese yam, golden cherry seed, Suanzaoren (fried), Shouwu Teng, Ligustrum lucidum, Dodder (made), Niu Dali, Poria, Mother of Pearl, Paeonia lactiflora (fried), Salvia, It is composed of 16 traditional Chinese medicines including Polygonum multiflorum, Polygonatum chinensis (system), Schisandra chinensis and Wuzhi Maotao, which is a compound preparation. It has the effect of nourishing the liver and kidney, calming the heart and soothing the mind, and is used for liver and kidney deficiency, dizziness and tinnitus, insomnia and dreaminess, dizziness and forgetfulness, backache leakage, neurasthenia and other symptoms. This variety is contained in the Ministry's "Pharmaceutical Standards" on page 340 of the 18th volume of traditi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/02G01N30/90
CPCG01N30/02G01N30/90
Inventor 韦智灵王永江郑文雅
Owner GUANGDONG YIHETANG PHARMA CO LTD
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