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Preparation method of quartz crucible mold

A mold and quartz technology, which is applied in the field of quartz clamp pot mold preparation, can solve the problems of complex crucible structure, high temperature resistance, easy damage, etc., and achieve the effects of simplifying the production process, increasing the strength, and improving the strength of the mold

Active Publication Date: 2018-05-04
SUZHOU HAOYAN PRECISION MOLD CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Molds are various molds and tools used in industrial production for blow molding, injection molding, extrusion or forging molding, smelting and other methods to obtain the required products. With the explosive growth of the photovoltaic market, the demand for crucibles is also increasing. At the same time, the size of the crucible is getting larger and larger, and the manufacture of the crucible requires the use of molds, but the structure of the traditional crucible mold is complex, not resistant to high temperature, and has poor strength and is easy to damage

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] The present embodiment provides a kind of preparation method of quartz pincer pot mould, specifically comprises the following steps:

[0023] Step 1: Send the fused silica sand with a purity of 99.99% and the fused silica sand with a purity of 99.995% to a ball mill respectively, adopt wet ball milling, and the ball milling time is 3.5 hours, and sieve through 70 mesh and 90 mesh respectively;

[0024] Step 2: Send the filler to the ball mill for dry ball milling. The ball milling time is 2.5 hours. The weight ratio of the filler to fused silica sand with a purity of 99.99% and fused silica sand with a purity of 99.995% is 1:9::7. And the filler includes the following components in parts by mass: zirconia: 9 parts, calcium carbonate: 10 parts, magnesium oxide: 4 parts, silicon carbide micropowder: 22 parts, bentonite: 13 parts, kaolin: 10 parts, calcite powder: 7 parts, barium sulfate: 5 parts, aluminum powder: 3 parts, nickel powder 1 part;

[0025] Step 3: Add fused ...

Embodiment 2

[0033] The present embodiment provides a kind of preparation method of quartz pincer pot mould, specifically comprises the following steps:

[0034] Step 1: Send the fused silica sand with a purity of 99.99% and the fused silica sand with a purity of 99.995% to a ball mill respectively, adopt a wet ball mill for 4 hours, and sieve through 70 mesh and 90 mesh respectively;

[0035] Step 2: send the filler to the ball mill, adopt dry ball milling, and the ball milling time is 3 hours, the weight ratio of the filler and the fused silica sand with a purity of 99.99% and the fused silica sand with a purity of 99.995% is 1:9::7, and The filler includes the following components in parts by mass: zirconia: 11 parts, calcium carbonate: 13 parts, magnesium oxide: 5 parts, silicon carbide micropowder: 24 parts, bentonite: 14 parts, kaolin: 12 parts, calcite powder: 8 parts Parts, barium sulfate: 6 parts, aluminum powder: 4 parts, nickel powder 2 parts;

[0036] Step 3: Add fused silica ...

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PUM

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Abstract

The invention discloses a preparation method of a quartz crucible mold. The preparation method specifically comprises the following steps: (1) grinding raw material components respectively and mixingand stirring according to the ratio; (2) injecting a mixture into a mold and adding filler; (3) drying in a vacuum drying box, wherein the vacuum degree is 0.08 to 0.09MPa, the drying temperature is 50 to 55 DEG C and the time is 2 to 4h; (4) putting the mixture into a heating furnace and heating by sections, wherein specific temperature is as follows: 200 to 260 DEG C, 350 to 420 DEG C and 550 to620 DEG C; (5) spraying and coating the filler; (6) sintering in a sintering furnace, wherein in a whole sintering flow technology, the time is 24 to 26h and the temperature is 1100 to 1220 DEG C. The quartz crucible mold disclosed by the invention has high strength, good wear resistance and high temperature resistance and the service life is prolonged.

Description

technical field [0001] The invention relates to a preparation method of a quartz clamp pot mold. Background technique [0002] Molds are various molds and tools used in industrial production for blow molding, injection molding, extrusion or forging molding, smelting and other methods to obtain the required products. With the explosive growth of the photovoltaic market, the demand for crucibles is also increasing. At the same time, the size of the crucible is also increasing, and the manufacture of the crucible requires the use of molds, but the structure of the traditional crucible mold is complex, not resistant to high temperatures, and has poor strength and is easily damaged. Contents of the invention [0003] The object of the present invention is to provide a kind of preparation method of quartz pincer pot mould. [0004] In order to achieve the above object, the present invention provides a technical solution as follows: a method for preparing a quartz clamp pot mold...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/14C04B35/622C04B41/87
CPCC04B35/14C04B35/622C04B41/009C04B41/5155C04B41/87C04B2235/3206C04B2235/3244C04B2235/349C04B2235/3826C04B2235/402C04B2235/405C04B2235/442C04B2235/448C04B2235/661C04B41/5144C04B41/5059C04B41/5042C04B41/5029C04B41/5037
Inventor 刘浩张君
Owner SUZHOU HAOYAN PRECISION MOLD CO LTD
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