Composite building humidity-controlling material and preparation method thereof
A humidity-adjusting material and construction technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of small air contact area, inconvenient and stable placement, etc., to achieve enhanced moisture absorption and desorption ability, fast moisture absorption and desorption rate , Promote the effect of physical adsorption
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example 1
[0025] Take 10g chitosan, add 1.0kg mass fraction of 2% acetic acid solution, stir at 300r / min until chitosan is completely dissolved, then add 1.0kg mass fraction of 5% benzaldehyde ethanol solution, and stir at 60°C 3h, after the reaction is finished, use a mass fraction of 5% sodium hydroxide solution to adjust the pH to 7, let it stand for 1h and filter to obtain a filter cake, wash the filter cake with absolute ethanol 3 times, then place the filter cake in a drying box, Dry to constant weight at 40°C to obtain N-benzylidene chitosan, take 10g N-benzylidene chitosan, 30mL isopropanol, add 150mL deionized water, stir at 300r / min for 20min, then add 10g of glycidyltrimethylammonium chloride, heat preservation reaction at 80°C for 6h, let stand for 1h after the reaction, and collect the filtrate by filtration, place the filtrate on a rotary evaporator and evaporate to dryness under reduced pressure to obtain a quaternized ammonium shell For polysaccharides, take 10g of quate...
example 2
[0027]Take 13g chitosan, add 1.2kg mass fraction of 2% acetic acid solution, stir at 350r / min until chitosan is completely dissolved, then add 1.2kg mass fraction of 5% benzaldehyde ethanol solution, and stir at 70°C 4h, after the reaction is finished, adjust the pH to 7.5 with a mass fraction of 5% sodium hydroxide solution, let it stand for 1h and filter to obtain a filter cake, wash the filter cake 4 times with absolute ethanol, then place the filter cake in a drying box, Dry to constant weight at 45°C to obtain N-benzylidene chitosan, take 11g N-benzylidene chitosan, 40mL isopropanol, add 175mL deionized water, stir at 350r / min for 25min, then add 11g of glycidyltrimethylammonium chloride, heat preservation reaction at 85°C for 7h, let stand for 1h after the reaction, and collect the filtrate by filtration, place the filtrate on a rotary evaporator and evaporate to dryness under reduced pressure to obtain a quaternized ammonium shell For polysaccharides, take 11g of quater...
example 3
[0029] Take 15g chitosan, add 1.5kg mass fraction of 2% acetic acid solution, stir at 400r / min until chitosan is completely dissolved, then add 1.5kg mass fraction of 5% benzaldehyde ethanol solution, and stir at 80°C 5h, after the reaction is finished, use a mass fraction of 5% sodium hydroxide solution to adjust the pH to 8, filter the filter cake after standing for 2 hours, wash the filter cake 5 times with absolute ethanol, then place the filter cake in a drying box, Dry at 50°C to constant weight to obtain N-benzylidene chitosan, take 12g N-benzylidene chitosan, 50mL isopropanol, add 200mL deionized water, stir at 400r / min for 30min, then add 12g of glycidyltrimethylammonium chloride, heat preservation reaction at 90°C for 8 hours, let stand for 2 hours after the reaction, and collect the filtrate by filtration, place the filtrate on a rotary evaporator and evaporate it to dryness under reduced pressure to obtain a quaternized ammonium shell For polysaccharides, take 12g ...
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