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A kind of preparation method of flow blocking agent for flame brazing or molten salt immersion brazing

A technology of dip brazing and flame brazing, used in welding equipment, manufacturing tools, welding media, etc., can solve the problems of stripping of flow blocking agent, decline of flow blocking effect, falling off, etc., and achieve good reaction inertness and strong resistance to molten salts. Corrosive effect

Active Publication Date: 2019-11-19
WENZHOU HONGFENG ELECTRICAL ALLOY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Existing flow blocking agents (such as NICROBRAZ Yellow Stop Off) need to increase the dosage to achieve a better flow blocking effect when dealing with brazing conditions that require the application of a large amount of flux or molten salt, but in molten salt environments, a large amount of The use of flow blocking agent will cause the flow blocking agent to peel off or fall off under the scouring of molten salt, resulting in a decrease in the flow blocking effect, and at the same time causing pollution to molten salt components

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] The choke agent for flame brazing or molten salt immersion brazing provided in this embodiment is composed of the following components by weight:

[0027] Cerium oxide powder: 2%

[0028] Alumina powder: 60%

[0029] Calcium fluoride powder: 3%

[0030] Chromium oxide powder: 25%

[0031] Potassium fluoroborate: 1%

[0032] Methylcellulose: 0.5%

[0033] Ethylene glycol: 2%

[0034] Hexene glycol: 6.5%

[0035] The particle size of the cerium oxide powder is between 15 microns and 45 microns, the particle size of the alumina powder is between 45 microns and 75 microns; the particle size of the calcium fluoride powder is between 15 microns and 45 microns ;The particle size of chromium oxide powder is between 45 microns and 75 microns;

[0036] The preparation method of the flow blocking agent comprises the following steps in turn:

[0037] (1) Weighing each component used to form the flow blocking agent by the aforementioned weight percentage;

[0038] (2) Add c...

Embodiment 2

[0044] The choke agent for flame brazing or molten salt immersion brazing provided in this embodiment is composed of the following components by weight:

[0045] Cerium oxide powder: 7%

[0046] Alumina powder: 35%

[0047] Calcium fluoride powder: 6%

[0048] Chromium oxide powder: 15%

[0049] Potassium fluoroborate: 5%

[0050] Methylcellulose: 0.15%

[0051] Ethylene glycol: 4%

[0052] Hexene glycol: 27.85%

[0053] The particle size of the cerium oxide powder is between 45 microns and 75 microns; the particle size of the alumina powder is between 15 microns and 45 microns; the particle size of the calcium fluoride powder is between 45 microns and 75 microns ;The particle size of chromium oxide powder is between 15 microns and 45 microns;

[0054] The preparation method of the flow blocking agent comprises the following steps in turn:

[0055] (1) Weighing each component used to form the flow blocking agent by the aforementioned weight percentage;

[0056] (2) Ad...

Embodiment 3

[0062] The choke agent for flame brazing or molten salt immersion brazing provided in this embodiment is composed of the following components by weight:

[0063] Cerium oxide powder: 5%

[0064] Alumina powder: 50%

[0065] Calcium fluoride powder: 4%

[0066] Chromium oxide powder: 20%

[0067] Potassium fluoroborate: 3%

[0068] Methylcellulose: 0.25%

[0069] Ethylene glycol: 3%

[0070] Hexene glycol: 14.75%

[0071] The particle size of the cerium oxide powder is between 25 microns and 55 microns; the particle size of the alumina powder is between 25 microns and 55 microns; the particle size of the calcium fluoride powder is between 25 microns and 55 microns ;The particle size of chromium oxide powder is between 25 microns and 55 microns;

[0072] The preparation method of the flow blocking agent comprises the following steps in turn:

[0073] (1) Weighing each component used to form the flow blocking agent by the aforementioned weight percentage;

[0074] (2) Add ...

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Abstract

The invention relates to the technical field of welding, and aims to provide a preparation method of a stopping-off agent for flame brazing or molten salt dip brazing. The preparation method comprisesthe steps as follows: cerium oxide powder and chromium oxide powder are subjected to ball-milling and then taken out, and a mixture I is obtained; aluminum oxide powder, calcium fluoride powder and potassium fluoborate are subjected to ball-milling, and a mixture II is obtained; after ethylene glycol and hexylene glycol are mixed and stirred uniformly, methyl cellulose is added and stirred uniformly, and a mixture III is obtained; the mixture I and the mixture II are added to the mixture III, and after stirring, a mixture IV is obtained; the mixture IV is added to a three-roll grinder for grinding and cooled to the room temperature, and the stopping-off agent for flame brazing or molten salt dip brazing is obtained. The stopping-off agent can be resistant to erosion of a molten brazing flux or molten salt in a brazing process, has quite good reactionlessness under the action of the molten brazing flux or molten salt and has better binding force with the surface of a workpiece in the brazing process, thereby having low probability of being washed away from the originally covered surface by the molten brazing flux or molten salt.

Description

technical field [0001] The invention relates to the field of welding technology, in particular to a preparation method of a flow blocking agent for flame brazing or molten salt dipping brazing. Background technique [0002] The anti-flow agent is a material used to protect the surface of the metal to be welded during the brazing process. It is a stable suspension system made by mixing oxides and binders. It can be formulated to have a suitable The composition of viscosity and rheological properties, its function is to effectively prevent the molten solder from flowing freely to the surface that does not need to be welded at the brazing temperature, and can be removed in a certain way after brazing without pollution and corrosion brazing metal. [0003] The flow blocking agent used in flame brazing or molten salt immersion brazing often needs to resist the erosion of molten flux and molten salt during brazing to ensure its own stability during use and not dissolve in molten ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B23K35/363
CPCB23K1/0002B23K35/361B23K35/362
Inventor 蔡伟炜张玲洁陈晓祁更新沈涛
Owner WENZHOU HONGFENG ELECTRICAL ALLOY
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