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Sewage treating agent and preparation method thereof

A technology of sewage treatment agent and room temperature water, which is applied in water/sewage treatment, water treatment parameter control, water/sludge/sewage treatment, etc. It can solve the problems of slow polymer flocculation, environmental impact, and high cost of biological treatment , to achieve good biocompatibility, increase the flocculation rate, and increase the flocculation rate

Inactive Publication Date: 2018-02-27
CHANGSHA QIUDIANBING INFORMATION TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, there are physical, chemical, biological, comprehensive and other methods to deal with the pollution of water resources, but most of the physical methods have problems of poor treatment effect and unstable treatment rate; the cost of biological methods is too high to be popularized and used; Chemical methods are used to treat sewage, but the existing sewage treatment agents have secondary pollution problems in their reagent components, which will also have a certain impact on the environment
Inorganic flocculant composite polymer has become the most researched flocculant at present. It has the characteristics of good flocculation effect and low toxicity, but the flocculation speed of the polymer part is slow, which leads to the unsatisfactory flocculation effect of the composite.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A kind of preparation method of sewage treatment agent, comprises the following steps:

[0022] S1. Add 0.8mol sodium acrylate and 0.4mol acrylamide to 1L water, bathe in water at room temperature, keep stirring at a speed of 500r / min and pass in nitrogen gas, add sodium hydroxide to adjust the pH value to 12.8, then add 0.0024mol dihydroxy diperiodide Acid copper (Ⅲ) potassium, the temperature of the water bath is raised to 68 ° C for 45 minutes, then add cooling and add hydrochloric acid with a mass fraction of 23% until the pH value of the solution is 4, continue to stir for 20 minutes, and wash with methanol and acetone alternately for 3 times. Dried to obtain a star polymer;

[0023] S2. In parts by weight, add 20 parts of tapioca starch to 1000 parts of water to gelatinize at 80°C, then lower the temperature to 55°C, add 1 part of sodium hydroxide, 5 parts of water-soluble cellulose, and 12 parts of S1 Prepared star polymer, 6 parts of acrylic acid, 21 parts of a...

Embodiment 2

[0025] A kind of preparation method of sewage treatment agent, comprises the following steps:

[0026] S1. Add 0.8mol sodium acrylate and 0.3mol acrylamide to 1L water, bathe in water at room temperature, keep stirring at a speed of 400r / min and pass in nitrogen gas, add sodium hydroxide to adjust the pH value to 13.5, then add 0.002mol dihydroxy diperiodide Acid copper (Ⅲ) potassium, the temperature of the water bath is raised to 66 ° C for 60 minutes, then add cooling and add hydrochloric acid with a mass fraction of 20% until the pH value of the solution is 3.5, continue to stir for 25 minutes, then wash with methanol and acetone alternately for 3 times, Dried to obtain a star polymer;

[0027] S2. In parts by weight, add 20 parts of tapioca starch to 1000 parts of water to gelatinize at 78°C, then lower the temperature to 52°C, add 1.3 parts of sodium hydroxide, 3 parts of water-soluble cellulose, and 11 parts of S1 Prepared star polymer, 8 parts of acrylic acid, 18 parts...

Embodiment 3

[0029] A kind of preparation method of sewage treatment agent, comprises the following steps:

[0030] S1. Add 0.8mol sodium acrylate and 0.5mol acrylamide to 1L water, bathe in water at room temperature, keep stirring at a speed of 300r / min and pass in nitrogen gas, add sodium hydroxide to adjust the pH to 13, then add 0.0028mol dihydroxy diperiodide Acid copper (Ⅲ) potassium, the temperature of the water bath is raised to 65 ° C for 50 minutes, then add cooling and add hydrochloric acid with a mass fraction of 25% until the pH value of the solution is 3, continue to stir for 23 minutes, then wash with methanol and acetone alternately for 3 times, Dried to obtain a star polymer;

[0031] S2. In parts by weight, add 20 parts of tapioca starch to 1000 parts of water to gelatinize at 83°C, then lower the temperature to 50°C, add 1.2 parts of sodium hydroxide, 6 parts of water-soluble cellulose, and 10 parts of S1 Prepared star polymer, 7 parts of acrylic acid, 23 parts of acryl...

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PUM

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Abstract

The invention discloses a sewage treating agent and a preparation method thereof. The preparation method comprises the following steps: firstly, preparing a star polymer by taking sodium acrylate andacrylamide as monomers and dihydroxyl diperiodiate potassium cuprate (III) as an initiator, then according to the weight parts, adding 20 parts of starch into 1000 parts of water, gelatinizing at 78-83 DEG C, then cooling the temperature to 50-55 DEG C, sequentially adding 1-1.3 parts of sodium hydroxide, 3-6 parts of cellulose, 10-12 parts of star polymer prepared in the S1, 6-8 parts of crylic acid, 18-23 parts of acrylamide, 0.35-0.38 parts of ammonium persulfate and 0.19-0.21 part of sodium sulfite, stirring for 20-30min, then adding 2-3 parts of an inorganic flocculant, and 0.032-0.045 part of N,N- methacrylamide, stirring for 30min and stopping reaction, then drying and grinding to obtain a sewage treatment agent. The prepared sewage treatment agent has the characteristics of fast flocculation speed, and low biodegradability and toxicity.

Description

technical field [0001] The invention relates to a sewage treatment agent and a preparation method thereof. Background technique [0002] Due to population growth and economic development, a series of problems affecting the quality of resources caused by excessive exploitation and irrational development and utilization of resources have directly threatened the survival of us and future generations. Our country is also facing these problems. Our country is a country with insufficient water resources and medical resources. How to alleviate the problems of water resource medical shortage and pollution has become an urgent problem. [0003] At present, there are physical, chemical, biological, comprehensive and other methods to deal with the pollution of water resources, but most of the physical methods have problems of poor treatment effect and unstable treatment rate; the cost of biological methods is too high to be popularized and used; Chemical methods are used to treat sewa...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F1/52
CPCC02F1/5245C02F1/5263C02F2209/10C02F2209/11
Inventor 卯志华
Owner CHANGSHA QIUDIANBING INFORMATION TECH CO LTD
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