Plant essence and preparation method thereof
A plant essence and extract technology, applied in the field of plant essence and its preparation, can solve the problems affecting skin respiration, achieve the effect of keeping the skin transparent, maintaining the balance of oil and water in the skin, and good water retention effect
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Embodiment 1
[0035] Embodiment one: a kind of preparation method of plant essence, comprises the steps:
[0036] 1. The preparation method of Selaginella extract: crush Selaginella, let it stand in 80% ethanol by volume fraction for 24 hours, keep the temperature at 60°C, and the volume ratio of Selaginella and 80% ethanol by volume fraction is 1:3, Obtain Selaginella extract;
[0037] Using ethanol with a volume fraction of 70% to extract the above Selaginella Selaginella again, and mix it with the Selaginella Selaginella extract to obtain the Selaginella Selaginella extract;
[0038] Silica gel is loaded into the chromatographic column, the Selaginella extract is poured into the chromatographic column, and 5% NaHCO is used successively 3 , 0.2% NaOH, chloroform-methanol mixed solvent (the volume ratio of chloroform and methanol is 8:1) and ethyl acetate-acetone-water (the volume ratio of ethyl acetate, acetone and water is 7:2.5:2.5) as washing Remove the agent, collect the Selaginella...
Embodiment 2
[0046] Embodiment two: a kind of preparation method of plant essence, comprises the steps:
[0047] 1. The preparation method of Selaginella extract: crush Selaginella, let it stand in 95% ethanol by volume fraction for 48h, keep the temperature at 80°C, and the volume ratio of Selaginella and 95% ethanol by volume fraction is 1:3, Obtain Selaginella extract;
[0048] Using ethanol with a volume fraction of 85% to extract the above Selaginella Selaginella again, and mix it with the Selaginella Selaginella extract to obtain the Selaginella Selaginella extract;
[0049] Silica gel is loaded into the chromatographic column, the Selaginella extract is poured into the chromatographic column, and 5% NaHCO is used successively 3 , 0.2% NaOH, chloroform-methanol mixed solvent (the volume ratio of chloroform and methanol is 9:1) and ethyl acetate-acetone-water (the volume ratio of ethyl acetate, acetone and water is 7:2.5:2.5) as washing Remove the agent, collect the Selaginella extr...
Embodiment 3
[0057] Embodiment three: a kind of preparation method of plant essence, comprises the steps:
[0058] 1. The preparation method of Selaginella extract: crush Selaginella, put it in ethanol with a volume fraction of 90% for 30 hours, keep the temperature at 70°C, and the volume ratio of Selaginella and ethanol with a volume fraction of 90% is 1:3, Obtain Selaginella extract;
[0059] Using ethanol with a volume fraction of 75% to extract the above Selaginella Selaginella again, and mix it with the Selaginella Selaginella extract to obtain the Selaginella Selaginella extract;
[0060] Silica gel is loaded into the chromatographic column, the Selaginella extract is poured into the chromatographic column, and 5% NaHCO is used successively 3 , 0.2% NaOH, chloroform-methanol mixed solvent (the volume ratio of chloroform and methanol is 9:1) and ethyl acetate-acetone-water (the volume ratio of ethyl acetate, acetone and water is 7:2.5:2.5) as washing Remove the agent, collect the S...
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