A kind of graphene/sodium alginate/carbon nanotube composite elastic aerogel for strain sensor and preparation method thereof
A carbon nanotube composite, strain sensor technology, applied in aerogel preparation, chemical instruments and methods, instruments, etc., can solve the problems of complex preparation process, unstable resistance, limiting the practical application of mixed aerogel, etc. The method is simple and practical, the resistance change is sensitive, and the effect of excellent strain sensing performance
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Embodiment 1
[0051] The preparation of the graphene / sodium alginate / carbon nanotube composite elastic airgel for strain sensor specifically includes the following steps:
[0052] (1) Place the prepared graphene oxide in deionized water, and adjust the concentration of the graphene oxide aqueous solution to 5 mg·mL -1 , sonicate for 2.5 h to disperse evenly; then sodium alginate (SA) solution (1 mg·mL -1 ), graphene oxide (GO) solution (1mg·mL -1 ) and carbon nanotubes (CNTs) suspension (1 mg·mL -1 ) was mixed according to the mass ratio GO:SA:CNTs=GO:SA:CNTs=20:7:3, and the mixture was stirred continuously at 140rpm for 3.5 hours, then put into a freeze dryer, and freeze-dried at -58°C for 48 hours. Obtain composite airgel;
[0053] (2) Then, the obtained composite airgel was placed in a tetrafluoroethylene reactor (ceramic microbeads were silicon nitride), and 4 N 2 ·H 2 Under O steam atmosphere, the reduction reaction was carried out at 100°C for 8 hours; after the reaction, it was...
Embodiment 2
[0055] The preparation of the graphene / sodium alginate / carbon nanotube composite elastic airgel for strain sensor specifically includes the following steps:
[0056] (1) Place the prepared graphene oxide in deionized water, and adjust the concentration of the graphene oxide aqueous solution to 3 mg•mL -1 , sonicate for 1.5 h to disperse evenly; then sodium alginate (SA) solution (3 mg·mL -1 ), graphene oxide (GO) solution (3mg·mL -1 ) and carbon nanotubes (CNTs) suspension (3mg·mL -1 ) After mixing according to the mass ratio GO:SA:CNTs=20:5:5, the mixture was continuously stirred at 130rpm for 2.5 hours, then put into a freeze dryer, and freeze-dried at -65°C for 48 hours to obtain a composite airgel;
[0057] (2) Then, the obtained composite airgel was placed in a tetrafluoroethylene reactor (ceramic microbeads were silicon nitride), and 4 N 2 ·H 2 Under O steam atmosphere, carry out the reduction reaction at 85°C for 10.5 hours; after the reaction, let it stand and ven...
Embodiment 3
[0059] The preparation of the graphene / sodium alginate / carbon nanotube composite elastic airgel for strain sensor specifically includes the following steps:
[0060] (1) Place the prepared graphene oxide in deionized water, and adjust the concentration of the graphene oxide aqueous solution to 4 mg•mL -1 , sonicated for 1h to disperse evenly; then sodium alginate (SA) solution (4mg·mL -1 ), graphene oxide (GO) solution (4mg·mL -1 ) and carbon nanotubes (CNTs) suspension (4mg·mL -1 ) After mixing according to the mass ratio GO:SA:CNTs=20:3:7, the mixture was continuously stirred at 150rpm for 2 hours, then put into a freeze dryer, and freeze-dried at -60°C for 48 hours to obtain a composite airgel;
[0061] (2) Then, the obtained composite airgel was placed in a tetrafluoroethylene reactor (ceramic microbeads were zirconia), and 4 N 2 ·H 2 Under O steam atmosphere, carry out reduction reaction at 90 DEG C for 10 hours; After the reaction is over, let it stand for ventilati...
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