Gaseous-phase antirust material with long-acting antirust effect and preparation method thereof
A gas-phase anti-rust, long-term technology, applied in the petroleum industry, lubricating compositions, etc., can solve the problems of insufficient anti-rust time, easy loss, dry cracking and brittleness, etc., achieve good oxidation resistance and storage stability, improve Anti-rust effect, effect of improving anti-rust ability
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Embodiment 1
[0039]Example 1 Preparation method of a long-term antirust gas phase antirust material
[0040] 1. Preparation of antirust microcapsules:
[0041] (1) Configure nano-titanium dioxide / gelatin composite solution:
[0042] Configure 4% gelatin solution, add 0.5% nano-titanium dioxide, and carry out high-speed emulsification and dispersion through a homogenizer at 2200r / min at a temperature of 65°C for 20 minutes to prepare a nano-titanium dioxide / gelatin composite liquid;
[0043] (2) Preparation of modified casein solution:
[0044] Add casein to distilled water and stir to form a paste, slowly add 0.15 mol / L NaOH solution until the casein is completely dissolved, and then boil for 5 minutes; dissolve succinate in ethanol to prepare a 10% succinate solution; The prepared succinate solution is dropped into the casein solution until the pH is 7.5-7.7, then stirred with a magnetic stirrer for 20 minutes at a temperature of 45°C, and then cooled to room temperature to make a modif...
Embodiment 2
[0059] Example 2 Preparation method of a long-term antirust gas phase antirust material
[0060] 1. Preparation of antirust microcapsules:
[0061] (1) Configure nano-titanium dioxide / gelatin composite solution:
[0062] Configure 3% gelatin solution, add 0.3% nano-titanium dioxide, and carry out high-speed emulsification and dispersion through a homogenizer at a temperature of 65°C for 15 minutes at a speed of 2000r / min to prepare a nano-titanium dioxide / gelatin composite liquid;
[0063] (2) Preparation of modified casein solution:
[0064] Add casein to distilled water and stir to form a paste, slowly add 0.13mol / L NaOH solution until the casein is completely dissolved, and then boil for 5 minutes; dissolve succinate in ethanol to prepare a 9% succinate solution; The prepared succinate solution was dropped into the casein solution until the pH was 7.7, then stirred with a magnetic stirrer for 10 minutes at a temperature of 45°C, and then cooled to room temperature to prep...
Embodiment 3
[0079] Example 3 Preparation method of a long-term antirust gas phase antirust material
[0080] 1. Preparation of antirust microcapsules:
[0081] (1) Configure nano-titanium dioxide / gelatin composite solution:
[0082] Configure 6% gelatin solution, add 0.8% nano-titanium dioxide, and carry out high-speed emulsification and dispersion through a homogenizer for 20 minutes at a speed of 2500r / min at a temperature of 70°C to prepare a nano-titanium dioxide / gelatin composite liquid;
[0083] (2) Preparation of modified casein solution:
[0084] Add casein to distilled water and stir to form a paste, slowly add 0.15 mol / L NaOH solution until the casein is completely dissolved, and then boil for 10 minutes; dissolve succinate in ethanol to prepare a 10% succinate solution; The prepared succinate solution was dropped into the casein solution until the pH was 7.7, then stirred with a magnetic stirrer for 20 minutes at a temperature of 50°C, and then cooled to room temperature to p...
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