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Subcritical injection method of grape seed anthocyanidins

A grape seed and anthocyanin technology, which is applied in the field of subcritical injection of grape seed anthocyanin, can solve the problems of high price and poor taste, and achieve the effect of low operating cost, large production capacity, and no damage to product activity

Active Publication Date: 2017-09-08
郑州郑大药食健康研究院有限公司 +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, anthocyanins are directly eaten after tedious extraction, refining and purification, the taste is poor, and the price is expensive

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] 200 g of dried grape seeds are crushed and passed through a 100-mesh sieve, placed in a subcritical extraction tank, vacuumed, and injected into the subcritical extraction tank with subcritical fluid dimethyl ether as an extraction solvent, grape seeds and extraction solvent The mass volume ratio of the mixture is 1:10 g / ml, the entrainer is ethanol solution with a volume fraction of 15%, the entrainment volume is 10%, the extraction time is 30 minutes, the temperature is 30°C, the pressure is 0.6 Mpa, and the extraction cycle is 4 times; After the extraction is finished, the liquid solvent is pumped into the evaporation tank, and the grape seeds and the liquid solvent are subjected to constant temperature desolventization treatment, and the liquid solvent is desolvated to obtain an extract containing grape seed anthocyanins.

[0027] Put the above extract and the commercially available Xinyang Maojian tea leaves into a subcritical injection tank at a mass ratio of 1:20 ...

Embodiment 2

[0030] 200 g of dried grape seeds are pulverized and passed through a 40-mesh sieve, placed in a subcritical extraction tank, vacuumed, and injected into the tank with subcritical fluid liquid ammonia for extraction as the extraction solvent, and the mass-to-volume ratio of the grape seeds to the extraction solvent is The entrainer is 1:30 g / ml, the entrainer is 95% ethanol solution, the entrainment amount is 1%, the extraction time is 10 minutes, the temperature is 40°C, the pressure is 0.1 MPa, and the extraction is repeated twice; after the extraction, the liquid solvent It is pumped into the evaporation tank, and the grape seeds and the liquid solvent are subjected to constant temperature desolventization treatment, and the liquid solvent is desolvated to obtain an extract containing grape seed anthocyanins.

[0031]Put the above extract and the commercially available Dahongpao tea leaves into a subcritical injection tank at a mass ratio of 1:30 g / g, inject a subcritical fl...

Embodiment 3

[0034] 100 g of dried grape seeds are pulverized and passed through a 60-mesh sieve, placed in a subcritical extraction tank, vacuumed, and injected into the tank with subcritical fluid dimethyl ether for extraction as the extraction solvent, the mass volume of the grape seeds and the extraction solvent The ratio is 1:15 g / ml, the entrainer is 50% ethanol solution, the entrainment amount is 5%, the extraction time is 15 minutes, the temperature is 35°C, the pressure is 0.58 Mpa, and the extraction is performed once; after the extraction, the liquid solvent Pumped into the evaporating tank, the grape seeds and the liquid solvent were subjected to constant temperature desolventization treatment, and the liquid solvent was desolvated to obtain 3.09 g of an extract containing grape seed anthocyanins.

[0035] Put the above extract and commercially available oatmeal into a subcritical injection tank at a mass ratio of 1:25 g / g, inject a subcritical fluid dimethyl ether into the tank...

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PUM

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Abstract

The invention relates to the field of subcritical extraction and injection, and particularly relates to a subcritical injection method of grape seed anthocyanidins, wherein the subcritical injection method is suitable for food, tobacco, medicine and food healthcare and other industries, has the advantages of simple process and low equipment investment, has relatively low pressure due to the fact that the whole process is performed under normal-temperature or low-temperature conditions, does not damage functional components of grape seed samples, anthocyanins and injected samples, and comprises the following steps: pretreating; sieving after drying and crushing; extracting; placing pretreated grape seeds into a subcritical extraction tank; injecting subcritical fluid as an extraction solvent; extracting under certain extraction conditions; desolventizing at a constant temperature and obtaining extracts containing the grape seed anthocyanidins after finishing extraction; placing the extracts and materials to be injected into a subcritical injection tank; adding an injection solvent; injecting under certain injection conditions; and desolventizing the injection tank at a constant temperature after finishing injection to obtain the materials after injection treatment.

Description

technical field [0001] The invention relates to the field of subcritical extraction and injection, and specifically relates to a method suitable for industries such as food, tobacco, medicine, food and health care. The process is simple and the investment in equipment is low. A subcritical injection method of grape seed anthocyanins that can damage grape seed samples, anthocyanins, and functional components injected into the samples. Background technique [0002] Grape seeds are rich in proanthocyanidins. Proanthocyanidins are polyphenol mixtures that widely exist in nature, and are mainly composed of catechin monomers, dimers, trimers, ... decamers, etc. Among them, the 2- to 5-mer is oligomeric proantho 2 cyanidin (OPC), which is famous for its high efficiency, low toxicity and high bioavailability. According to reports, OPC has a strong antioxidant capacity. In the body, its ability to resist oxidation and scavenge free radicals is 50 times that of Ve and 20 times that...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D11/02A23F3/14A23L7/143A23L33/105A61K31/352A61P39/06A61P9/00A61P9/10A61P1/16A61P9/14A61P27/10A61P27/02
CPCA23F3/14A23L7/143A23L33/105A23V2002/00A61K31/352B01D11/02B01D11/0288A23V2200/30A23V2200/326A23V2250/21166
Inventor 谷令彪陈忠华宋晓龙
Owner 郑州郑大药食健康研究院有限公司
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