conductive ink
A conductivity and ink technology, applied in the direction of conductive pattern formation, ink, conductive materials dispersed in non-conductive inorganic materials, etc., can solve problems such as complicated steps
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preparation example 1
[0147] 8.9 g of 3-methoxypropylamine (reagent grade 1 manufactured by Wako Pure Chemical Industries, Ltd., carbon number: 4, logP: -0.5), and 0.3 g of Dispa as a polymer dispersant DISPERBYK-111 was mixed and fully stirred with a magnetic stirrer to generate an amine mixture (relative to the silver, the molar ratio of the added amine was 10). Then, while stirring, 3.0 g of silver oxalate was added. After silver oxalate was added, stirring was continued at room temperature, whereby the silver oxalate was changed into a viscous white substance, and the change was visually confirmed to be complete in appearance, and the stirring was terminated at this point (the first step).
[0148] The obtained mixed solution was transferred to an oil bath, and heated and stirred at 120°C. Immediately after starting the stirring, the reaction accompanied by the generation of carbon dioxide was started, and then the stirring was continued until the generation of carbon dioxide was completed, t...
preparation example 2
[0151] 8.9 g of 3-methoxypropylamine (reagent grade 1 manufactured by Wako Pure Chemical Industries, Ltd., carbon number: 4, logP: -0.5), and 0.3 g of Dispa as a polymer dispersant DISPERBYK-102 was mixed and fully stirred with a magnetic stirrer to generate an amine mixture (relative to silver, the molar ratio of the added amine was 5). Then, while stirring, 3.0 g of silver oxalate was added. After silver oxalate was added, stirring was continued at room temperature, whereby the silver oxalate was changed into a viscous white substance, and the change was visually confirmed to be complete in appearance, and the stirring was terminated at this point (the first step).
[0152] The obtained mixed solution was transferred to an oil bath, and heated and stirred at 120°C. Immediately after starting the stirring, the reaction accompanied by the generation of carbon dioxide was started, and then the stirring was continued until the generation of carbon dioxide was completed, thereb...
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