Wet process production technology for sodium pyrosulfite

A sodium pyrosulfite and production process technology, which is applied in the field of wet process production of sodium pyrosulfite, can solve the problems of inability to popularize and apply, many impurity components, and low purity, and achieve the effects of repeated utilization, simplified preparation process, and flexible use

Inactive Publication Date: 2017-08-25
金昌正旭工贸有限责任公司
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  • Summary
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Problems solved by technology

[0004] In the traditional production and processing method of sodium metabisulfite, two methods of dry method and wet method are adopted. At the same time of dry method production and processing, soda ash and water are mixed according to a certain ratio, and then sulfur dioxide gas is introduced to make the reaction to prepare the finished product, but The finished product prepared by dry method contains many impurities and the purity is not high, so it cannot be further popularized and applied when some production needs
For the wet preparation process, often due to a large amount of energy consumption, the production cost is greatly increased, and the purity of the preparation is low, and it cannot be used as a further application

Method used

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Examples

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Effect test

Embodiment

[0022] The present embodiment provides a kind of wet production process of sodium pyrosulfite, and the operation process is as follows:

[0023] 1) preparation of sulfur dioxide: burning sulfur to make sulfur dioxide, after cooling and washing, set aside;

[0024] Send the sulfur flakes into the combustion furnace, and use the air compressor to inject air into the sulfur combustion furnace. The amount of air added is about 2 times the theoretical amount, and the combustion is carried out at 600-800°C to obtain a gaseous sulfur dioxide concentration of 9%-11%. The gaseous sulfur dioxide is filtered to remove dust and cooled and washed to remove sublimed sulfur and other acidic impurities, so that the temperature of the gas is reduced to about 50°C, and then it is passed into the reactor. The small amount of filtered impurities produced in this process is mainly composed of sublimated elemental sulfur, which is collected and sent to the combustion furnace for repeated combustion...

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PUM

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Abstract

The invention provides a wet production process of sodium pyrosulfite, which is characterized in that the operation process is as follows: 1) preparation of sulfur dioxide: burning sulfur to make sulfur dioxide, which is cooled and washed for later use; 2) preparation of sodium sulfite solution: using Low-content sodium sulfite preparation solution; 3) Preparation of sodium pyrosulfite crystals: add sulfur dioxide to the solution prepared in step 2), and precipitate sodium pyrosulfite crystals; 4) Preparation of sodium pyrosulfite: Centrifuge the sodium pyrosulfite crystals, and recycle the sodium sulfite solution , and dry the sodium metabisulfite crystals. Through the preparation method provided by the present invention, low-content sodium sulfite is directly used to produce sodium pyrosulfite, which greatly shortens the process flow, makes the wet production process of sodium pyrosulfite save the waste of raw material resources, realizes effective production, increases enterprise income, and is more applicable In the current industrialized large-scale production and processing.

Description

technical field [0001] The invention relates to the field of sodium sulfite, in particular to a wet production process of sodium pyrosulfite. Background technique [0002] Sodium sulfite is common sulfite, monoclinic crystal or powder. It is irritating to eyes, skin and mucous membranes, and can pollute water sources. Decomposition by high heat produces toxic sulfide fumes. [0003] Sodium pyrosulfite is white or yellow crystalline powder or small crystals with a strong smell of sulfur dioxide. Sodium pyrosulfite has a wide range of biological uses in industry. It can be used in the purification of chloroform, coagulant, deoxidizer, mordant, in pharmaceutical technology, rubber preparation Food grade sodium metabisulfite can be used as leavening agent and preservative in various aspects of life. [0004] In the traditional production and processing method of sodium metabisulfite, two methods of dry method and wet method are adopted. At the same time of dry method producti...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01D5/14
CPCC01D5/145
Inventor 安鹏九
Owner 金昌正旭工贸有限责任公司
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