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Forging process for preparing isotropic ultrahigh-strength heat-resistant magnesium alloy structural member

An isotropic, magnesium alloy technology, applied in the field of multi-directional forging deformation of Mg-Gd-Y-Zr magnesium alloys, can solve the problems of uneven structure and mechanical properties, anisotropy of mechanical properties, and small anisotropy. , to avoid excessive grain growth, high mechanical properties, and small anisotropy

Active Publication Date: 2017-08-11
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The reasons are as follows: first, the addition of rare earths such as Gd and Y increases the deformation resistance of the magnesium alloy and narrows the processing window; second, due to factors such as friction, the sample has a difficult and easy deformation zone during free forging, and the deformation is not stable. Uniform and difficult to penetrate, resulting in uneven structure and mechanical properties; third, magnesium alloy has a special hexagonal close-packed structure, and the deformation process is very easy to produce texture, resulting in obvious anisotropy of mechanical properties
These three reasons make it difficult to prepare large-scale Mg-Gd-Y-Zr forgings with uniform structure, up-to-standard performance and small anisotropy

Method used

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  • Forging process for preparing isotropic ultrahigh-strength heat-resistant magnesium alloy structural member
  • Forging process for preparing isotropic ultrahigh-strength heat-resistant magnesium alloy structural member
  • Forging process for preparing isotropic ultrahigh-strength heat-resistant magnesium alloy structural member

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] The semi-continuous electromagnetic casting method is used to prepare ingots with a diameter of φ400mm and a length of 2500mm. The composition is Mg-8.65Gd-2.43Y-0.28Ag-0.16Er-0.38Zr (wt.%). , Machining an ingot with a diameter of φ380mm and a length of 830mm. After homogenizing annealing at 490°C for 20h, it was cooled to room temperature with the furnace. Before forging, heat the heat preservation ingot billet at 510°C for 10 hours, heat the upper and lower flat anvils to 325°C, and perform multi-pass multi-directional forging at a slow speed of 10mm / s on a vertical hydraulic press. The two radial directions are Z, Y and X directions respectively; firstly carry out 3 times of upsetting along the Z, Y and X directions, the deformation of each pass is 40%, and press the cylindrical blank into a hexahedron; then Y or X is the axis, rolling and compressing the edges and corners for 5 passes, the deformation amount of each pass is 30%, and the hexahedron is pressed into a...

Embodiment 2

[0027] Semi-continuous electromagnetic casting was used to prepare an ingot with a diameter of φ450mm, a length of 2300mm, and a composition of Mg-8.72Gd-2.84Y-0.22Ag-0.11Er-0.31Zr (wt.%). After casting, it was kept at 225°C for 14h for stress relief annealing , machined an ingot with a diameter of φ420mm and a length of 930mm. For details, see figure 1. Homogenized annealing at 520°C for 18 hours, and then cooled to room temperature with the furnace. Before forging, heat the ingot at 490°C for 16 hours, heat the flat anvil to 350°C, and perform multi-pass multi-directional forging at a slow speed of 8mm / s on a vertical hydraulic press. The radial directions are Z, Y and X directions respectively; first, 6 times of upsetting are carried out along the Z, Y and X directions, and the deformation amount of each pass is 30%, and the cylindrical blank is pressed into a hexahedron; then Y or X is used as the Shaft, rolling and compressing the edges and corners 6 times, the deformat...

Embodiment 3

[0029] Semi-continuous electromagnetic casting was used to prepare an ingot with a diameter of φ450mm, a length of 2300mm, and a composition of Mg-8.94Gd-2.94Y-0.18Ag-0.10Er-0.45Zr (wt.%). After casting, it was kept at 240°C for 14h to relieve stress and anneal. , machined an ingot with a diameter of φ420mm and a length of 1020mm. For details, see figure 1 . Homogenized annealing at 500°C for 20 hours, and then cooled to room temperature with the furnace. Heat the ingot at 520°C for 10 hours before forging, heat the flat anvil to 300°C, and perform multi-pass multi-directional forging at a slow speed of 8mm / s on a vertical hydraulic press after being out of the furnace. The two radial directions are Z, Y and X directions respectively; first, 6 times of upsetting are carried out along the Z, Y and X directions, and the deformation amount of each pass is 25%, and the cylindrical blank is pressed into a hexahedron; then Y or X is the axis, rolling and compressing the edges and ...

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Abstract

The invention discloses a forging process for preparing an isotropic ultrahigh-strength heat-resistant magnesium alloy structural member. Firstly, a cast ingot prepared through semi-continuous electromagnetic casting is subjected to homogenizing annealing, an ingot blank is formed through machining, the height direction of the cylindrical ingot blank and any two mutually perpendicular radial directions are used as the Z direction, the Y direction and the X direction correspondingly, 3-6 passes of heading are performed in the Z direction, the Y direction and the X direction, and the pass deformation amount is 20-40%; then the X direction or the Y direction is used as the axis, 2-6 passes of corner angle rolling compressing are performed, the pass deformation amount is 10-20%, intermediate annealing is performed, and the forging process is performed repeatedly once or twice; a forge piece is subjected to T6 treatment after forging is finished, and a final forge piece with the diameter being 450-650 mm and the height being 300-700 mm is obtained; as for both the height direction and the radial directions of the T6 state at the room temperature, the tensile strength is larger than or equal to 460 MPa, the yield strength is larger than or equal to 400 MPa, the ductility is larger than or equal to 4%, and the strength difference between the height direction and the radial directions is smaller than or equal to 10 MPa, and the ductility difference between the height direction and the radial direction is smaller than or equal to 0.5%; and as for both the height direction and the radial directions at the temperature of 200 DEG C, the tensile strength is larger than or equal to 350 MPa, and the ductility is larger than or equal to 6%.

Description

technical field [0001] The invention relates to the field of thermal deformation of high-strength heat-resistant magnesium alloys, in particular to multidirectional forging deformation of Mg-Gd-Y-Zr series magnesium alloys. Background technique [0002] Magnesium alloy has the advantages of large reserves, low density, high specific strength and specific stiffness, and is known as "green material in the 21st century". Compared with die castings, wrought magnesium alloys have gained more and more applications due to their special advantages. Deformed magnesium alloys can obtain ideal shapes and sizes through deformation, and can also use deformation to eliminate casting defects, refine grains, and improve mechanical properties. As a typical wrought magnesium alloy, Mg-Gd-Y-Zr alloy has attracted wide attention for its excellent mechanical properties and heat resistance. At present, the application of Mg-Gd-Y-Zr alloy is still mainly extruded profiles and rolled plates, and ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C23/06C22F1/06
CPCC22C23/06C22F1/06
Inventor 刘楚明王必正蒋树农高永浩陈志永万迎春
Owner CENT SOUTH UNIV
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