Preparation method for amorphous alloy/pure copper layered composite material
A technology of layered composite materials and amorphous alloys, applied in the field of materials, can solve problems affecting the overall mechanical properties of composite materials, crystallization of amorphous alloys at the interface, and complex processes
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Embodiment 1
[0018] The preparation method of amorphous alloy / pure copper layered composite material, its step comprises:
[0019] Step 1: Zr 41.2 Ti 13.8 Ni 10 Cu 12.5 be 22.5 Amorphous alloy adopts high-vacuum non-consumable arc melting furnace to melt master alloy, spray cast into Zirconium-based bulk amorphous alloy rods; Zr-based bulk amorphous alloy rods and copper The sample was smoothed with 1200# sandpaper, and the upper and lower surfaces of the amorphous sample and the copper sample were guaranteed to be parallel to each other; then it was placed in acetone and alcohol for 5 minutes of ultrasonic vibration cleaning, in order to reduce the influence of oxygen atoms on the interface, after drying Immediately put into the vacuum autoclave;
[0020] Step 2: Pump high vacuum to 10 -5 Pa, and then heated to the hot pressing temperature of 370°C at a heating rate of 40k / min, with a deformation rate of 10 -3 the s -1 down, will Zirconium-based bulk amorphous alloy rods ...
Embodiment 2
[0022] The preparation method of amorphous alloy / pure copper layered composite material, its step comprises:
[0023] Step 1: Zr 41.2 Ti 13.8 Ni 10 Cu 12.5 be 22.5 Amorphous alloy adopts high-vacuum non-consumable arc melting furnace to melt master alloy, spray cast into Zirconium-based bulk amorphous alloy rods; Zr-based bulk amorphous alloy rods and copper The sample was smoothed with 1200# sandpaper, and the upper and lower surfaces of the amorphous sample and the copper sample were guaranteed to be parallel to each other; then it was placed in acetone and alcohol for 5 minutes of ultrasonic vibration cleaning, in order to reduce the influence of oxygen atoms on the interface, after drying Immediately put into the vacuum autoclave;
[0024] Step 2: Pump high vacuum to 10 -4 Pa, and then heated to the hot pressing temperature of 390°C at a heating rate of 40k / min, with a deformation rate of 10-3s-1, the Zirconium-based bulk amorphous alloy rods were diffusion-...
Embodiment 3
[0026] The preparation method of amorphous alloy / pure copper layered composite material, its step comprises:
[0027] Step 1: Zr 41.2 Ti 13.8 Ni 10 Cu 12.5 be 22.5 Amorphous alloy adopts high-vacuum non-consumable arc melting furnace to melt master alloy, spray cast into Zirconium-based bulk amorphous alloy rods; Zr-based bulk amorphous alloy rods and copper The sample was smoothed with 1200# sandpaper, and the upper and lower surfaces of the amorphous sample and the copper sample were guaranteed to be parallel to each other; then it was placed in acetone and alcohol for 5 minutes of ultrasonic vibration cleaning, in order to reduce the influence of oxygen atoms on the interface, after drying Immediately put into the vacuum autoclave;
[0028] Step 2: Pump high vacuum to 10 -3 Pa, and then heated to the hot pressing temperature of 400°C at a heating rate of 40k / min, with a deformation rate of 10 -3 the s -1 down, will Zirconium-based bulk amorphous alloy rods ...
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