Lithium-sodium-potassium codoped dental microcrystalline glass and preparation method and application thereof
A technology of glass-ceramic and sodium-potassium, applied in dental preparations, dentistry, dental prostheses, etc., to achieve the effects of easy-to-obtain raw materials, stable process, and simple raw materials
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Embodiment 1
[0043] According to the ratio of each component in Table 1, a certain amount of analytically pure raw material (SiO 2 , Li 2 CO 3 、Na 2 CO 3 、K 2 CO 3 , NH 4 h 2 PO 4 and ZrO 2 ), use a ball mill to mix evenly for 8 hours; then put the powder into a platinum crucible, place it in the air atmosphere of a box-type resistance furnace, and heat it at 4°C / min to 330°C and 850°C for 1 hour each to remove nitrogen and carbon , continue to heat up to 1500°C and keep it warm for 1 hour; then, take out the crucible, pour the melt into deionized water to quench, and dry to obtain fragments of glass melt; ball mill again, and the powder is directly heated to 1500°C / 1 hour for remelting ;Cast the remelted molten glass into a mold preheated at 550°C, quickly put it into a resistance furnace, heat it at 500°C for 10 minutes, then immediately rise to 550°C and hold it for 30 minutes, then cool with the furnace. The cast glass block is first subjected to nucleation at 620°C / 1 hour an...
Embodiment 2
[0045] According to the ratio of each component in Table 1, a certain amount of analytically pure raw material (SiO 2 , Li 2 CO 3 、Na 2 CO 3 、K 2 CO 3 , NH 4 h 2 PO 4 and ZrO 2 ), use a ball mill to mix evenly for 8 hours; then put the powder into a platinum crucible, place it in the air atmosphere of a box-type resistance furnace, and heat it at 4°C / min to 330°C and 850°C for 1 hour each to remove nitrogen and carbon , continue to heat up to 1500°C and keep it warm for 1 hour; then, take out the crucible, pour the melt into deionized water to quench, and dry to obtain fragments of glass melt; ball mill again, and the powder is directly heated to 1500°C / 1 hour for remelting ;Cast the remelted molten glass into a mold preheated at 550°C, quickly put it into a resistance furnace, heat it at 500°C for 10 minutes, then immediately rise to 550°C and hold it for 30 minutes, then cool with the furnace. The cast glass block is first subjected to nucleation at 610°C / 1 hour an...
Embodiment 3
[0047] According to the ratio of each component in Table 1, a certain amount of analytically pure raw material (SiO 2 , Li 2 CO 3 、Na 2 CO 3 、K 2 CO 3 , NH 4 h 2 PO 4 and ZrO 2 ), use a ball mill to mix evenly for 8 hours; then put the powder into a platinum crucible, place it in the air atmosphere of a box-type resistance furnace, and heat it at 4°C / min to 330°C and 850°C for 1 hour each to remove nitrogen and carbon , continue to heat up to 1500°C and keep it warm for 1 hour; then, take out the crucible, pour the melt into deionized water to quench, and dry to obtain fragments of glass melt; ball mill again, and the powder is directly heated to 1500°C / 1 hour for remelting ;Cast the remelted molten glass into a mold preheated at 550°C, quickly put it into a resistance furnace, heat it at 500°C for 10 minutes, then immediately rise to 550°C and hold it for 30 minutes, then cool with the furnace. The cast glass block is first subjected to nucleation at 590°C / 1 hour, a...
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