A method for preparing 2,6-dichlorotoluene by catalyzing o-chlorotoluene with ionic liquid
An ionic liquid, dichlorotoluene technology, applied in chemical instruments and methods, physical/chemical process catalysts, preparation of halogenated hydrocarbons, etc., can solve the problems of difficulty in product separation and purification, low comprehensive yield, difficulty in selecting chlorination, etc., Achieve the effect of good industrial application value, high conversion rate of raw materials, and easy product separation
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[0020] The present invention will be described in further detail below in conjunction with specific embodiments.
[0021] A method for preparing 2,6-dichlorotoluene by selective chlorination of o-chlorotoluene comprises the following steps:
[0022] 1) Preparation of ionic liquid [BMIM]Cl-2AlCl 3 Under the protection of N 2, 0.65 mol of 1-methylimidazole and 0.7 mol of chloro-n-butane were stirred and mixed in a 250 mL three-necked flask with a condenser, and the temperature was increased. The reaction was carried out under reflux at 80°C for 48h. The product was separated by a separatory funnel, the unreacted liquid was removed, and the product was washed three times with 20 mL of ethyl acetate. The crude product was subjected to rotary evaporation under vacuum at 60°C to remove residual ethyl acetate, and vacuum-dried at 70°C for 24 h. The obtained pale yellow liquid was the intermediate of [BMIM]Cl ionic liquid, which was stored in a dry N2 atmosphere for later use.
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