Iron-copper alloy powder and preparation method thereof
A technology of iron-copper alloy and pre-alloyed powder, which is applied in the field of iron-copper alloy powder and its preparation, which can solve the problems of poor cold press formability, low bulk density, and high green strength, and achieve low bulk density and make up for loose bulk density. The effect of high density and high green strength
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Embodiment 1
[0055] (1) Copper powder is prepared by a water atomization method, and the prepared copper powder is roasted and crushed to obtain copper oxide powder with a particle diameter not greater than 75 μm, and the oxygen content in the copper oxide powder is 16%;
[0056] (2) adopt water atomization method to prepare iron-copper pre-alloy powder, wherein copper content is 10%, and iron content is 90%;
[0057] (3) The copper oxide powder prepared in step (1) and the iron-copper pre-alloy powder prepared in step (2) are added to the double cone mixer according to the mass ratio of copper oxide powder 30%, iron-copper pre-alloy powder 70% In the feeder, mix evenly for 48min to prepare the iron-copper powder precursor;
[0058] (4) the iron-copper powder precursor that is prepared in step (3) is placed in the N that volume ratio is 1:3 2 and H 2 The sintering is carried out in a mixed gas, the sintering temperature is set to 600°C, and the sintering time is 2h, so as to realize the ...
Embodiment 2
[0061] (1) Copper powder is prepared by a water atomization method, and the prepared copper powder is roasted and crushed to obtain copper oxide powder with a particle diameter not greater than 75 μm, and the oxygen content in the copper oxide powder is 17%;
[0062] (2) adopt water atomization method to prepare iron-copper pre-alloy powder, wherein copper content is 20%, and iron content is 80%;
[0063] (3) The copper oxide powder prepared in step (1) and the iron-copper pre-alloy powder prepared in step (2) are added to the double cone mixer according to the mass ratio of copper oxide powder 10%, iron-copper pre-alloy powder 90% In the feeder, mix evenly for 50 minutes to prepare the iron-copper powder precursor;
[0064] (4) the iron-copper powder precursor that is prepared in step (3) is placed in the N that volume ratio is 1:4 2 and H 2 The sintering is carried out in the mixed gas, the sintering temperature is set to 400°C, and the sintering time is 1.5h, so as to rea...
Embodiment 3
[0067] (1) Copper powder is prepared by a water atomization method, and the prepared copper powder is roasted and crushed to obtain copper oxide powder with a particle diameter not greater than 75 μm, and the oxygen content in the copper oxide powder is 20%;
[0068] (2) adopt water atomization method to prepare iron-copper pre-alloy powder, wherein copper content is 30%, and iron content is 70%;
[0069] (3) the copper oxide powder prepared in step (1) and the iron-copper pre-alloy powder prepared in step (2), according to copper oxide powder 20%, the mass ratio of iron-copper pre-alloy powder 80% is added to double cone mixer In the feeder, mix evenly for 40 minutes to prepare the iron-copper powder precursor;
[0070] (4) the iron-copper powder precursor that is prepared in step (3) is placed in the N that volume ratio is 1:5 2 and H 2 The sintering is carried out in the mixed gas, the sintering temperature is set to 850°C, and the sintering time is 3.5h, so as to realize...
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