Method of preparing ultrathin silicide
A silicide, ultra-thin technology, used in semiconductor/solid-state device manufacturing, semiconductor devices, electrical components, etc., can solve the problems of secondary annealing temperature not too high, different annealing temperatures in different regions, interface spikes, etc. The effect of requirements, low cost and simple process
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[0029] The present invention will be described in detail below in conjunction with the accompanying drawings and specific examples.
[0030] Process flow of the present invention such as figure 1 As shown, the preparation of ultra-thin nickel silicide can be realized according to the following steps:
[0031] 1) ALD on a 4-inch N-type (100) bulk silicon substrate Al 2 o 3 As an insertion barrier, such as figure 2 shown;
[0032] 2) Sputter 50nm metallic Ni. Such as image 3 shown;
[0033] 3) Perform rapid thermal annealing at 600°C for 10 minutes, metal Ni diffuses through the insertion barrier layer and reacts with silicon to form NiSi 2 ,Such as Figure 4 shown;
[0034] 4) Use the ratio of H 2 SO 4 :H 2 o 2 = 4:1 solution to remove unreacted Ni and Al 2 o 3 , the corrosion time is 10min, such as Figure 5 shown;
[0035] Ultimately achieve ultra-thin NiSi with a thickness of less than 2nm 2 preparation.
[0036] The embodiments of the present inventio...
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