Preparation method of stable-type odor-free low-density foam concrete foamer
A foamed concrete and low-density technology, applied in the field of concrete foaming agents, can solve the problems of unsuitability for low-density foamed concrete, unsatisfactory foaming ratio, poor foam stability, etc., and achieves simple process, easy operation and high foaming efficiency. Effect
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example 1
[0017] Weigh 100g of humic acid, pour it into a beaker filled with 1L of 8% sodium hydroxide solution, and then place the beaker in a digital speed measuring constant temperature magnetic stirrer at a temperature of 55°C and a speed of 350r / min. Under constant temperature, stir and mix for 45min, filter, remove the filter residue, collect the No. 1 filtrate, then add dropwise hydrochloric acid with a mass fraction of 8%, adjust the pH of the No. 1 filtrate to 2.0, let stand for 8h, filter, remove the filter residue, and collect the No. 2 filtrate Measure 200mL of the above-mentioned obtained No. 2 filtrate, add in a three-necked flask with a stirrer, then add dropwise a mass fraction of 10% sodium hydroxide solution, adjust the pH to 10.2, then add 5g of octadecyltrimethylammonium chloride , at a temperature of 60°C and a rotation speed of 300r / min, stir and react at a constant temperature for 3 hours, then transfer the material in the three-neck flask to a rotary evaporator, a...
example 2
[0020]Weigh 200g of humic acid, pour it into a beaker filled with 2L of 10% sodium hydroxide solution, and then place the beaker in a digital speed measuring constant temperature magnetic stirrer at a temperature of 65°C and a speed of 450r / min. Stir and mix at constant temperature for 60 minutes, filter, remove the filter residue, collect No. 1 filtrate, then add dropwise hydrochloric acid with a mass fraction of 10%, adjust the pH of No. 1 filtrate to 2.2, let stand for 12 hours, filter, remove the filter residue, and collect No. 2 filtrate Measure 300mL of the No. 2 filtrate of the above-mentioned gained, add in the there-necked flask with agitator, then add dropwise a mass fraction of 15% sodium hydroxide solution, adjust the pH to 10.5, then add 8g of octadecyltrimethylammonium chloride , at a temperature of 65°C and a speed of 400r / min, stir and react at a constant temperature for 5 hours, then transfer the material in the three-necked flask to a rotary evaporator, and co...
example 3
[0023] Weigh 150g of humic acid, pour it into a beaker filled with 2L of 9% sodium hydroxide solution, and then place the beaker in a digital speed measuring constant temperature magnetic stirrer at a temperature of 60°C and a speed of 400r / min. Under constant temperature, stir and mix for 53 minutes, filter, remove the filter residue, collect the No. 1 filtrate, then add dropwise the mass fraction of 9% hydrochloric acid, adjust the pH of the No. 1 filtrate to 2.1, let it stand for 10 hours, filter, remove the filter residue, and collect the No. Measure 250mL of the above-mentioned obtained No. 2 filtrate, add in the there-necked flask with agitator, then add dropwise a mass fraction of 13% sodium hydroxide solution, adjust the pH to 10.4, then add 7g of octadecyltrimethylammonium chloride , at a temperature of 63°C and a speed of 350r / min, stir and react at a constant temperature for 4 hours, then transfer the material in the three-necked flask to a rotary evaporator, and con...
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