A kind of low-density ablative thermal insulation composite material and preparation method thereof
A composite material and low-density technology, applied in the field of carbon materials, can solve the problems of restricting large-scale production, harsh process conditions, and long preparation cycle
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Embodiment 1
[0042] A certain amount of prepared thermosetting phenolic resin and curing agent-paraformaldehyde were respectively weighed, added into a reaction kettle containing a certain amount of ethanol, and mechanically stirred until completely dissolved to obtain a phenolic resin solution. Wherein the mass ratio of phenolic resin to ethanol is 1:20, and the mass ratio of phenolic resin to paraformaldehyde is 20:1.
[0043] Set the density to 150Kg / m 3 The polypropylene-based carbon fiber felt was cut into a size of 150mm×150mm, and placed in a 100°C oven for heat treatment for more than 6 hours; the heat-treated carbon fiber felt was laid flat in a stainless steel mold customized by the laboratory, and the above-mentioned phenolic resin solution was used in the Slowly impregnate the carbon fiber felt under normal temperature and pressure until the phenolic resin impregnating solution can completely soak the carbon fiber felt, then seal the mold, place it in an oven at 80°C, undergo a...
Embodiment 2
[0045] A certain amount of prepared thermosetting phenolic resin and curing agent-hexamethylenetetramine were respectively weighed, added into a reaction kettle containing a certain amount of ethanol, and mechanically stirred until completely dissolved to obtain a phenolic resin solution. Wherein the mass ratio of phenolic resin to ethanol is 1:10, and the mass ratio of phenolic resin to hexamethylenetetramine is 10:1.
[0046] Set the density to 150Kg / m 3 The polypropylene-based carbon fiber felt was cut into a size of 150mm×150mm, and placed in a 100°C oven for heat treatment for more than 6 hours; the heat-treated carbon fiber felt was laid flat in a stainless steel mold customized by the laboratory, and the above-mentioned phenolic resin solution was used in the Slowly impregnate the carbon fiber felt under normal temperature and pressure until the phenolic resin impregnating solution can completely soak the carbon fiber felt, then seal the mold, place it in an oven at 80°...
Embodiment 3
[0048] A certain amount of prepared thermosetting phenolic resin and curing agent-paraformaldehyde were respectively weighed, added into a reaction kettle containing a certain amount of ethanol, and mechanically stirred until completely dissolved to obtain a phenolic resin solution. Wherein the mass ratio of phenolic resin to ethanol is 1:2, and the mass ratio of phenolic resin to paraformaldehyde is 5:1.
[0049] Set the density to 150Kg / m 3 The polypropylene-based carbon fiber felt was cut into a size of 150mm×150mm, and placed in a 100°C oven for heat treatment for more than 6 hours; the heat-treated carbon fiber felt was laid flat in a stainless steel mold customized by the laboratory, and the above-mentioned phenolic resin solution was used in the Slowly impregnate the carbon fiber felt under normal temperature and pressure until the phenolic resin impregnating solution can completely soak the carbon fiber felt, then seal the mold, place it in an oven at 80°C, undergo a s...
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