A kind of preparation method of long-acting conductive polyester fiber
A polyester fiber and long-acting technology, which is applied in the field of preparation of long-acting conductive polyester fibers, can solve the problems of reduced conductive durability, poor compactness, and poor material compactness, and achieve enhanced conductive durability and compactness, and high conductive durability , The effect of easy processing and molding
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example 1
[0018]First, weigh 200g of mussel meat, manually chop it, transfer it to a colloid mill, and grind it for 15 minutes to obtain minced mussel meat, then add it to a beaker filled with 1L of deionized water, and add 6% sodium hydroxide dropwise Adjust the pH of the solution to 7.6, then add 0.8 g of alkaline protease, and then transfer the beaker to a magnetic stirrer with a digital display speed measurement and a constant temperature. Under the conditions of a temperature of 60 ° C and a rotation speed of 380 r / min, stir and react at a constant temperature for 3 hours, and then heat up to 90°C, inactivate the enzyme for 8 minutes, centrifuge, discard the lower sediment to obtain the supernatant; then measure 300mL of the above-obtained supernatant, add it to a beaker filled with 200mL deionized water, and then place the beaker in a water bath for magnetic On the stirrer, adjust the temperature of the water bath to 45°C, and the stirring speed to 300r / min. Under stirring, add 180...
example 2
[0021] First, weigh 250g of mussel meat, manually chop it, transfer it to a colloid mill, and grind it for 18 minutes to obtain minced mussel meat, then add it to a beaker filled with 2L of deionized water, and add 7% sodium hydroxide dropwise Adjust the pH of the solution to 7.7, then add 1.0 g of alkaline protease, and then transfer the beaker to a magnetic stirrer with a digital display speed measurement and a constant temperature. Under the condition of a temperature of 63 ° C and a rotation speed of 420 r / min, the reaction is stirred at a constant temperature for 4 hours, and then the temperature is raised to 93°C, inactivate the enzyme for 10 minutes, centrifuge, discard the lower sediment to obtain the supernatant; then measure 350mL of the above-obtained supernatant, add it to a beaker filled with 250mL deionized water, and then place the beaker in a water bath magnetically On the stirrer, adjust the temperature of the water bath to 48°C, and the stirring speed to 350r / ...
example 3
[0024] First, weigh 300g of mussel meat, manually chop it, transfer it to a colloid mill, and grind it for 20 minutes to obtain minced mussel meat, then add it to a beaker filled with 2L deionized water, and add 8% sodium hydroxide dropwise Adjust the pH of the solution to 7.8, then add 1.2 g of alkaline protease, and then transfer the beaker to a digital display speed measuring constant temperature magnetic stirrer, at a temperature of 65 ° C and a speed of 460 r / min, stir and react at a constant temperature for 5 hours, then heat up to 95°C, inactivate the enzyme for 12 minutes, centrifuge, discard the lower sediment to obtain the supernatant; then measure 400mL of the above-obtained supernatant, add it to a beaker filled with 300mL deionized water, and then place the beaker in a water bath for magnetic On the stirrer, adjust the temperature of the water bath to 50°C, and the stirring speed to 400r / min. Under stirring, add 200mL of zinc chloride solution with a mass fraction ...
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