Photo chromic resin composite material and preparation method thereof

A resin composite material and photochromic technology, applied in the field of resin materials, can solve the problems of affecting service life and antibacterial effect, difficult to achieve effect, easy to agglomerate, etc., and achieve excellent formaldehyde removal performance, good antibacterial effect, and long-term antibacterial effect. active effect

Inactive Publication Date: 2017-01-18
佛山市高明区尚润盈科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in the existing methods, metal ions such as nano-silver and matrix resin cannot be tightly combined (especially when the content of nano-silver particles increases, agglomeration is prone to occur), and it is easy to fall off during use, thereby affecting the service life and antibacterial effect.
At the same time, the existing resin materials have a single function, and one resin material cannot meet various needs. Often, resin materials with multiple functions are mixed, but it is difficult to achieve the desired effect.

Method used

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  • Photo chromic resin composite material and preparation method thereof
  • Photo chromic resin composite material and preparation method thereof
  • Photo chromic resin composite material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A kind of preparation method of antibacterial composite material, it comprises the following steps:

[0028] (1) Preparation of graphene quantum dot suspension: weigh 0.5g of C60 powder, measure 50ml of concentrated sulfuric acid with a mass fraction of 98%, mix C60 powder and concentrated sulfuric acid in a beaker, place the beaker in an ice-water bath, and simultaneously Stir at a speed of 500rpm to obtain a mixed solution; weigh 3g of potassium permanganate powder, and slowly add it to the above mixed solution; remove the ice-water bath and replace it with a water bath, keep the temperature of the water bath at 30~40°C, and react for 8 hours; quickly add 200ml of pure Water, filtered, and then dialyzed for 3 days with a dialysis bag with a molecular weight cut-off of 1000 to obtain a suspension of graphene quantum dots; the suspension of graphene quantum dots was stirred at a speed of 100 rpm, while laser irradiation was performed for 30 minutes, and the laser irradia...

Embodiment 2

[0037] A kind of preparation method of antibacterial composite material, it comprises the following steps:

[0038] (1) Preparation of graphene quantum dot suspension: Weigh 0.7g of C60 powder, measure 80ml of concentrated sulfuric acid with a mass fraction of 98%, mix C60 powder and concentrated sulfuric acid in a beaker, place the beaker in an ice-water bath, and simultaneously Stir at a speed of 500rpm to obtain a mixed solution; weigh 2g of potassium permanganate powder, and slowly add it to the above mixed solution; remove the ice-water bath and replace it with a water bath, keep the temperature of the water bath at 30-40°C, and react for 6 hours; quickly add 200ml of pure Water, filtered, and then dialyzed for 3 days with a dialysis bag with a molecular weight cut-off of 1000 to obtain a suspension of graphene quantum dots; the suspension of graphene quantum dots was stirred at a speed of 100 rpm, while laser irradiation was performed for 45 minutes, and the laser irradia...

Embodiment 3

[0047] A kind of preparation method of antibacterial composite material, it comprises the following steps:

[0048] (1) Preparation of graphene quantum dot suspension: Weigh 0.8g of C60 powder, measure 100ml of concentrated sulfuric acid with a mass fraction of 98%, mix C60 powder and concentrated sulfuric acid in a beaker, put the beaker in an ice-water bath, and simultaneously Stir at a speed of 500rpm to obtain a mixed solution; weigh 1g of potassium permanganate powder, and slowly add it to the above mixed solution; remove the ice-water bath and replace it with a water bath, keep the temperature of the water bath at 30-40°C, and react for 5 hours; quickly add 100ml of pure Water, filtered, and then dialyzed for 3 days with a dialysis bag with a molecular weight cut-off of 1000 to obtain a suspension of graphene quantum dots; the suspension of graphene quantum dots was stirred at a speed of 100 rpm, while laser irradiation was performed for 60 minutes, and the laser irradiat...

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Abstract

The invention discloses a photo chromic resin composite material and preparation thereof. The method comprises the steps of 1, pretreating the pan macro porous adsorption resin by amination; 2, adding the pan macro porous adsorption resin processed in step 1 into diatomaceous earth or porous carbon dispersed solution, conducting ultrasonic agitation and static drying for using; 3, adding antibacterial composite material dispersion solution, conducting ultrasonic agitation and static drying for using; 4, adding photo chromic composite dispersion, conducting ultrasonic agitation and static drying, so that the photo chromic resin composite material is obtained. As the result of the reasonable collocation of diatomite, photo chromic compounds and antibacterial composite material, the resin material has excellent antibacterial properties, formaldehyde removal properties, and photo chromic properties with the synergistic effect of the three. The resin material meet the demand of multifunctional resin materials, thereby further broadening the application of resin materials.

Description

technical field [0001] The invention relates to the technical field of resin materials, in particular to a photochromic resin composite material and a preparation method thereof. Background technique [0002] At present, antibacterial materials prepared by various metal ions have become a research hotspot, such as the preparation of new broad-spectrum antibacterial functional fibers by chemical modification of organic polypropylene nitrile fibers, and metal complexed broad-spectrum antibacterial functional fibers. However, in the existing methods, metal ions such as nano-silver cannot be tightly combined with the matrix resin (especially when the content of nano-silver particles increases, agglomeration is prone to occur), and it is easy to fall off during use, thereby affecting the service life and antibacterial effect. At the same time, the existing resin materials have a single function, and one resin material cannot meet various needs. Often, resin materials with multipl...

Claims

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Application Information

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IPC IPC(8): C08L33/20C08K13/06C08K9/12C08K7/24C08K7/26C08K3/22C08K3/36C08K3/04C08K9/00C08K9/10C08K3/08C08K9/02C08F8/32C08F20/44
CPCC08K13/06C08F8/32C08K3/04C08K3/08C08K3/22C08K3/36C08K7/24C08K7/26C08K9/00C08K9/02C08K9/10C08K9/12C08K2003/0806C08K2003/221C08K2003/2213C08K2003/2241C08K2003/2296C08K2201/011C08F20/44C08L33/20
Inventor 陆庚
Owner 佛山市高明区尚润盈科技有限公司
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