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Preparation method for biological steel reinforcement corrosion inhibitor

A steel bar rust inhibitor and biological technology, which is applied in the field of embroidery inhibitor preparation, can solve the problems that the steel bar rust inhibitor cannot be well diffused, the steel bar corrosion inhibition effect is poor, and the antirust ability is poor, so as to achieve good inhibition effect and prevent Good rust ability and prolonging the life of steel structure

Inactive Publication Date: 2016-11-09
陈毅忠
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention: Aiming at the disadvantages that the current steel bar rust inhibitor cannot be well diffused in concrete, so when it is used for the repair of concrete structure, it has poor inhibitory effect on steel bar corrosion, poor anti-rust ability and large usage amount, provides A kind of fresh dinoflagellates is crushed, soaked in citrate buffer solution, filtered and dried to obtain a dried product for later use, then mixed with Dunaliella salina powder, zinc oxide and citric acid and filtered to obtain a filtrate and a filter residue, the filter residue is washed, dried, rinsed The liquid and the filtrate are mixed and concentrated to obtain a concentrated liquid for future use, and after drying, the filter residue is mixed with the dry matter for use, gluconic acid, etc., and then mixed with the concentrated liquid and calcium chloride solution to obtain a mixed liquid, etc. to prepare a biological steel rust inhibitor.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0016] First, weigh 200g of fresh dinoflagellates, clean the surface, put them in an oven and dry them for 5 hours at 50°C, after drying, crush and sieve to obtain 100 mesh dinoflagellate powders, and mix the powders with a solid-to-liquid ratio of 1:5 and a pH of 7.4 Mix the citrate buffer solution, soak for 2 hours, filter to obtain the filter residue, and put it in an oven to dry at 40°C to obtain the dried product, which is set aside; then weigh 150g of Dunaliella salina powder, 10g of zinc oxide powder and 2g of citric acid , put it into the reaction kettle after stirring and mixing, add 2L deionized water into the reaction kettle, set the temperature of the reaction kettle to 280°C, seal and stir the reaction for 1h at this temperature, cool to room temperature after the reaction, and filter the reactants to obtain Filter residue and filtrate, filter residue was rinsed with petroleum ether for 2 times and then dried in an oven, then the rinse liquid and filtrate were mixe...

example 2

[0019] First, weigh 225g of fresh dinoflagellates, clean the surface and put them in an oven to dry for 7 hours at 55°C. After drying, they are crushed and sieved to obtain dinoflagellate powder of 110 mesh. 7.4 Mix the citrate buffer solution, soak for 3 hours, filter to obtain the filter residue, and put it in an oven to dry at 43°C to obtain the dried product for later use; then weigh 175g of Dunaliella salina powder, 11g of zinc oxide powder and 3g of citric acid , put it into the reaction kettle after stirring and mixing, add 3L deionized water into the reaction kettle, set the temperature of the reaction kettle to 290°C, seal and stir the reaction at this temperature for 2h, cool to room temperature after the reaction, and filter the reactants to obtain Filter residue and filtrate, filter residue was rinsed with petroleum ether for 3 times and then put into an oven to dry, then the rinse solution and filtrate were mixed, put into a separatory funnel and let stand in layer...

example 3

[0022] First, weigh 250g of fresh dinoflagellates, clean the surface, put them in an oven and dry them at 60°C for 8 hours, crush them after drying, and sieve them to get 120 mesh dinoflagellates powder. 7.4 Mix the citrate buffer solution, soak for 3 hours, filter to obtain the filter residue, and put it in an oven to dry at 45°C to obtain the dried product for later use; then weigh 200g of Dunaliella salina powder, 12g of zinc oxide powder and 3g of citric acid , put it into the reaction kettle after stirring and mixing, add 3L deionized water into the reaction kettle, set the temperature of the reaction kettle to 300°C, seal and stir the reaction for 2h at this temperature, cool to room temperature after the reaction, and filter the reactants to obtain Filter residue and filtrate, filter residue was rinsed with petroleum ether for 3 times and then put into an oven to dry, then the rinse liquid and filtrate were mixed, put into a separatory funnel and let stand in layers to g...

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Abstract

The invention discloses a preparation method for a biological steel reinforcement corrosion inhibitor, and belongs to the technical field of preparation of corrosion inhibitors. The method comprises the following steps: crushing and impregnating fresh flagellates in a citrate buffer solution, performing filtration and drying to obtain a dried product for later use, mixing dunaliella salina powder, zinc oxide and citric acid for reaction, performing filtration to obtain filtrate and filter residues, mixing a flushing fluid and the filtrate, performing concentration to obtain a concentrated solution for later use, mixing and filtering the filter residues, the dried product obtained for later use, gluconic acid and the like after drying, and mixing a product, a mixed solution prepared from the concentrated solution and a calcium chloride solution and the like to obtain the biological steel reinforcement corrosion inhibitor. The preparation method has the beneficial effects that the preparation steps are simple; the steel reinforcement corrosion inhibitor is prepared from the flagellates, and is safe, nontoxic and high in corrosion inhibition capability; after the biological steel reinforcement corrosion inhibitor is used, the steel reinforcement corrosion inhibition effect is good, the using amount is reduced by 15.6 to 18.3 percent, corrosion to steel reinforcement is retarded, and the service life of a steel reinforcement structure is prolonged by 5 to 8 years.

Description

technical field [0001] The invention relates to a preparation method of a biological steel bar rust inhibitor, belonging to the technical field of embroidery inhibitor preparation. Background technique [0002] Steel bar rust inhibitor, an admixture mixed into concrete to prevent or slow down the corrosion of steel bars. Steel bar rust inhibitor refers to chemical substances added to concrete or painted on the surface of concrete to prevent or slow down the corrosion of steel bars. Some additives or external coating protective agents that can improve the protective performance of concrete on steel bars do not belong to the category of steel bar rust inhibitors. Steel bar rust inhibitors must be able to directly prevent or delay steel bar corrosion. Its types include anodic steel rust inhibitor, cathodic steel rust inhibitor and composite steel steel rust inhibitor. The anode-type steel bar rust inhibitor acts on the anode area, and inhibits the steel bar corrosion by preve...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B24/00C04B103/61
CPCC04B40/0039C04B24/00C04B2103/61
Inventor 陈毅忠盛海丰王统军
Owner 陈毅忠
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