A Statistical Method for Identifying {110} Crystal Planes and Surface Shares of Tungsten Single Crystal Coatings
A {110}, statistical method technology, applied in the field of thermionic fuel cells, can solve the problems of limiting the electrochemical etching process parameters, such as the thermoelectric conversion efficiency of the emitter coating, and achieve the statistical method is simple and easy to operate, simple and convenient to operate, and convenient Statistical effect of facet share
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[0025] Weigh 10g NaOH and 10g K respectively successively 3 Fe(CN) 6 Reagent, placed in a beaker, slowly add 100ml deionized water (20°C) into the beaker while stirring, and use ultrasonic waves to make NaOH and K 3 Fe(CN) 6 All solid reagents are dissolved and used as corrosive solution. Put the polished cylindrical tube with tungsten single crystal coating in the corrosion solution, and take it out after 30s. Rinse with deionized water and wipe clean with a cotton dampened with alcohol. Then observe with a metallographic microscope, take the first metallographic photo at the position of 0° along the circumference of the cylindrical tube, and then take the second metallographic photo at the position of 3°, successively at 6°, 9°, 12°,..., 354° , Take the 3rd, 4th, 5th, ..., 119th, and 120th metallographic photos at 357°, in which the topography of incomplete diamond-shaped pits is as follows figure 1 As shown, it is the {110} crystal plane; the morphology of the trapezoi...
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