A method for preparing high specific capacity shuttle-shaped copper oxide electrode material
A copper oxide, shuttle-like technology, used in hybrid capacitor electrodes, copper oxide/copper hydroxide, nanotechnology, etc., can solve the problems of limited use, high cost, toxicity, etc., and achieve narrow particle size distribution, broad application prospects, Responsive and efficient effect
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Embodiment 1
[0035] First need to weigh 1mmol CuCl 2 , into a 50mL beaker, then add 40mL deionized water, stir, then add 1mmol Na 2 CO 3 and 1mL of triethylamine solution, stirred for 10 minutes, then ultrasonicated for 5 minutes, and then directly put into the microwave oven, set the power to 300W, and the time was 20 minutes, and washed several times with deionized water and absolute ethanol, and then in Dry in an oven at 60°C for 6 hours to obtain a copper oxide nanoshuttle sample. Such as figure 1 Shown product is identified as copper oxide through X-ray powder diffraction; Carry out morphology analysis to copper oxide with scanning electron microscope (SEM), from figure 2 It can be seen that its morphology is nanoshuttle. Excellent electrochemical cycle performance and specific capacitance can be obtained from image 3 see.
Embodiment 2
[0037] First need to weigh 1mmol CuCl 2 , into a 50mL beaker, then add 40mL deionized water, stir, then add 1mmol Na 2 CO 3 and 1mL of triethylamine solution, stirred for 10 minutes, then ultrasonicated for 5 minutes, and then directly put into the microwave oven, set the power to 200W, and the time was 20 minutes, and washed several times with deionized water and absolute ethanol, and then in Dry in an oven at 60°C for 6 hours to obtain a copper oxide nanoshuttle sample. The morphology of copper oxide was analyzed by transmission electron microscopy (TEM). Figure 4 It can be seen that its morphology is nanoshuttle.
Embodiment 3
[0039] First need to weigh 1mmol CuCl 2 , into a 50mL beaker, then add 40mL deionized water, stir, then add 1mmol Na 2 CO 3 and 1mL of triethylamine solution, stirred for 10 minutes, then ultrasonicated for 5 minutes, and then directly put into the microwave oven, set the power to 400W, and the time was 20 minutes, and washed several times with deionized water and absolute ethanol, and then in Dry in an oven at 60°C for 6 hours to obtain a copper oxide nanoshuttle sample. The morphology of copper oxide was analyzed by transmission electron microscopy (TEM). Figure 5 It can be seen that its morphology is nanoshuttle.
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