Electrostatic self-assembly deepening method for fabric
An electrostatic self-assembly and fabric technology, applied in dyeing, animal fiber, textiles and papermaking, etc., can solve the problems of complex process, reduction, and many steps, and achieve the effect of simple preparation, changing interaction, and easy industrial production
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[0023] (1) Preparation of darkening agent A: weigh polyethyleneimine (PEI), and ultrasonically disperse and dilute it with deionized water to form a PEI aqueous solution with a mass fraction of 0.05%-0.2%;
[0024] (2) Preparation of deepening agent B: use deionized water to make the nano-silica sol solution into an aqueous dispersion with a mass fraction of silicon dioxide of 5%-15%;
[0025] (3) Deepening treatment: process the dyed silk fabric according to the following procedures, first soak it in darkening agent A for 5 minutes, take it out, wash it with deionized water for 2-4 times, each time for 2 minutes, and then immerse it in darkening agent B After soaking for 5 minutes, wash it with pure water for 2-4 times, each time for 2 minutes, so as to complete a cycle of assembly, and repeat the above process to complete the assembly of the film, so as to achieve the effect of deepening the fabric.
Embodiment 1
[0027] First weigh 0.4g of PEI with a purity of 50% with an electronic balance, set the volume to a 100mL volumetric flask, and disperse evenly by ultrasonication for 10 minutes to obtain a 0.2% PEI aqueous solution (deepening agent A) for use.
[0028] Take 50nmSiO 2 15g of sol solution is placed in a beaker, 95g of high-purity water is placed in a separatory funnel, the magnetic stirrer is adjusted to a suitable speed, the rate of dropping of high-purity water in the separatory funnel is controlled at a rate of 1 drop / second, and the concentration of silicon dioxide obtained is 15% SiO 2 Aqueous dispersion (Darkener B).
[0029] Deepening treatment: the dyed silk fabric is treated according to the following procedures, first soaked in PEI aqueous solution for 5 minutes, then taken out, washed with deionized water for 4 times, each time for 2 minutes, and then immersed in SiO 2 After soaking in the water dispersion for 5 minutes, wash with deionized water for 4 times, each ...
Embodiment 2
[0032] Weigh 0.2 g of PEI with a purity of 50% with an electronic balance, set volume to a 100 mL volumetric flask, and disperse evenly by ultrasonication for 10 min to obtain a PEI aqueous solution with a concentration of 0.1% for use.
[0033] First take 100nmSiO 2 Put 10g of sol solution in a beaker, place 92g of high-purity water in a separatory funnel, adjust the magnetic stirrer to a suitable speed, control the dropping rate of high-purity water in the separatory funnel at a rate of 1 drop / second, and prepare a concentration of 10% SiO 2 water dispersion.
[0034] Darkening treatment: The dyed silk fabric is treated according to the following procedures, first soaked in PEI aqueous solution for 5 minutes, then taken out, washed with deionized water for 3 times, each time for 2 minutes, and then immersed in SiO 2After immersing in the water dispersion for 5 minutes, wash with deionized water for 3 times, each time for 2 minutes, so as to complete one cycle of assembly, r...
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