Preparing method of super-hydrophilicity titanium dioxide hollow micro-nanospheres
A technology of titanium dioxide and micro-nano spheres, applied in the field of photocatalytic materials, can solve problems such as energy consumption, unfavorable practical application, damage, etc., and achieve the effect of avoiding human body damage
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[0023] In order to achieve the above purpose, the technical scheme adopted in the preparation method of a hydrophilic titanium dioxide hollow micro-nanosphere of the present invention is: introducing a template agent and a chelating complexing agent into the hydrothermal reaction system to induce the directional deposition and regulation of titanium ions The growth mode of the titanium dioxide crystal growth unit is to obtain titanium dioxide micro-nanospheres with a hollow structure and broad-spectrum response characteristics after the inner core is removed by calcination. The specific steps are:
[0024] 1) Using self-made monodisperse polystyrene spheres with negative charges on the surface as a template, the polystyrene sphere template and TiCl 3 The aqueous solution is mixed, and then a certain amount of potassium persulfate is added as a chelating complexing agent, and then transferred into a hydrothermal reaction kettle.
[0025] 2) Seal and mark the reaction kettle, p...
Embodiment 1
[0033] Take 0.2 g of polystyrene balls with a diameter of 700 nm and 0.15 mol / L of TiCl 3 90 mL of the aqueous solution was mixed under the condition of 800 r / min magnetic stirring, and then 1 g of potassium persulfate was added. Transfer the above mixed solution into a 100mL hydrothermal reaction kettle lined with tetrafluoroethylene, seal and mark. The above reaction kettle was put into a drying oven preheated to 200°C in advance, and kept at 200°C for 3 hours to carry out hydrothermal reaction. After naturally cooling to room temperature, the solid product in the reactor was washed several times with deionized water, and then dried at 60°C. Put the dried sample into a muffle furnace, raise the temperature to 500°C at a rate of 4°C / min and keep it for 6 hours, then raise it to 600°C at a rate of 1°C / min and keep it for 3 hours, and finally obtain a titanium dioxide hollow microstructure. ball structure.
Embodiment 2
[0035] The only difference from Example 1 is that the consumption of potassium persulfate is 0.4g.
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