Compression-resistant and wear-resistant lubricating agent
A lubricant, molybdenum disulfide technology, applied in the field of compressive and wear-resistant lubricants, can solve the problems affecting the application of nano-molybdenum disulfide, easy to agglomerate, difficult to disperse, etc.
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Embodiment 1
[0019] 90 parts by weight of base oil, 2.5 parts by weight of polymethacrylate, 3 parts by weight of phosphobisoctyl basic zinc salt, 1.8 parts by weight of trihydroxybenzoic acid, 1 part by weight of dienyl succinyl The phenylalanine of imine, 1.5 parts by weight, the calcium sulfonate of 0.8 parts by weight, the graphite powder of 2 parts by weight, the modified molybdenum disulfide of 2.5 parts by weight, the naphthyl phenyl phosphate of 2.0 parts by weight and 1.2 parts by weight parts of polyvinyl n-propyl ester.
[0020] Concrete preparation operation is:
[0021] Step 1: Take by weighing 2g ammonium molybdate, 1.5g sulfur powder and 7.5ml glycerol 180 ℃ of mixing reaction 2h, after reaction finishes, extract reaction product with toluene, reclaim lower floor solution, wash and dry with water and make molybdenum disulfide Use; Next, mix 1ml of tetraethoxy silicon with 25ml of absolute ethanol, then add 2.5ml of triethanolamine, 1.8mL of distilled water and 0.12g of hexa...
Embodiment 2
[0026] 95 parts by weight of base oil, 2.0 parts by weight of polymethacrylate, 3.5 parts by weight of thiophosphobisoctyl basic zinc salt, 1.5 parts by weight of trihydroxybenzoic acid, 1.5 parts by weight of dienyl succinyl The phenylalanine of imine, 1.2 parts by weight, the calcium sulfonate of 1.2 parts by weight, the graphite powder of 1.2 parts by weight, the modified molybdenum disulfide of 3.0 parts by weight, the naphthyl phenyl phosphate of 1.8 parts by weight and 1.5 parts by weight parts of polyvinyl n-propyl ester.
[0027] Concrete preparation operation is:
[0028] Weigh 2g of ammonium molybdate, 1.5g of sulfur powder and 7.5ml of glycerin and mix and react for 2h at 180°C. After the reaction, extract the reaction product with toluene, reclaim the lower layer solution, wash and dry with water to obtain molybdenum disulfide for use; Mix 1ml of tetraethoxy silicon with 25ml of absolute ethanol, then add 2.5ml of triethanolamine, 1.8mL of distilled water and 0.12...
Embodiment 3
[0033] A pressure-resistant and wear-resistant lubricant, the composition of which is as follows: 90-95 parts by weight of base oil, 2.8-3 parts by weight of polymethacrylate, 3-3.5 parts by weight of basic zinc salt of phosphobisoctyl, 1-1.2 parts by weight of trihydroxybenzoic acid, 1-1.5 parts by weight of dienyl succinimide, 0.8-1 parts by weight of phenylalanine, 1-1.5 parts by weight of calcium sulfonate, 0.8-1.2 parts by weight Graphite powder in parts by weight, modified molybdenum disulfide in 3.2-3.5 parts by weight, naphthyl phenyl phosphate in 2-2.5 parts by weight and polyvinyl n-propyl ester in 1.5-1.8 parts by weight.
[0034] Concrete preparation operation is:
[0035] Weigh 2g of ammonium molybdate, 1.5g of sulfur powder and 7.5ml of glycerin and mix and react for 2h at 180°C. After the reaction, extract the reaction product with toluene, reclaim the lower layer solution, wash and dry with water to obtain molybdenum disulfide for use; Mix 1ml of tetraethoxy s...
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