Preparation method of novel magneto-electric coupling multi-ferroic material BiMn3Cr4O12
A magnetoelectric coupling, multiferroic technology, applied in the field of materials science, can solve the problems of limited and restricted novelty effect research and application, achieve high critical temperature, good application prospects, large dielectric constant and electric polarization strength Effect
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Embodiment 1
[0026] Bi with a purity higher than 99.9% 2 o 3 , Mn 2 o 3 and Cr 2 o 3 After fully grinding at a molar ratio of 1:3:4, pass through a 200-mesh sieve; put the screened raw materials into gold or platinum capsules and compact them, wherein the gold or platinum capsules have a diameter of 10 mm and a length of 10 mm. The wall thickness is 2mm; the gold or platinum capsule is placed in a six-sided top press or a 6-8 type two-stage pusher press, and the pressure is set at 8GPa and the temperature is 1050°C, so that the raw materials in the gold or platinum capsule are under high temperature and high pressure. The reaction time was 30 minutes.
[0027] figure 1 The novel magnetoelectric coupling multiferroic material BiMn prepared by embodiment 1 is shown 3 Cr 4 o 12 The XRD pattern. Via a novel magnetoelectrically coupled multiferroic material BiMn 3 Cr 4 o 12 The XRD pattern of the prepared BiMn can be obtained 3 Cr 4 o 12 It belongs to the A-site ordered cubic do...
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