a bi 1‑x re x feo 3 /cofe 2 o 4 Multiferroic composite film and preparation method thereof
A composite film and multiferroic technology, applied in the manufacture of inductors/transformers/magnets, the magnetism of inorganic materials, electrical components, etc., can solve the problems of large leakage current and weak magnetism, and achieve improved ferroelectric performance and high magnetic permeability rate, the effect of large magnetocrystalline anisotropy
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Embodiment 1
[0039] Step 1, Co(NO 3 ) 2 ·6H 2 O and Fe(NO 3 ) 3 9H 2 O was dissolved in the mixture of ethylene glycol methyl ether and acetic anhydride, and stirred for 2 hours to obtain uniformly mixed CoFe 2 o 4 Precursor, CoFe 2 o 4 The concentration of Co ions in the precursor solution is 0.1mol / L, and the volume ratio of ethylene glycol methyl ether and acetic anhydride is 3:1;
[0040] Step 2, the Bi(NO 3 ) 3 ·5H 2 O, Ce(NO 3 ) 3 ·6H 2 O and Fe(NO 3 ) 3 9H 2 O is dissolved in a mixture of ethylene glycol methyl ether and acetic anhydride at a molar ratio of 0.90:0.15:1 (RE=Ce, x=0.15, excess bismuth nitrate), and stirred for 2 hours to obtain a uniformly mixed Bi 0.85 Ce 0.15 FeO 3 Precursor, Bi 0.85 Ce 0.15 FeO 3 The total concentration of metal ions in the precursor solution is 0.3mol / L, and the volume ratio of ethylene glycol methyl ether and acetic anhydride is 3:1;
[0041] Step 3, the prepared CoFe 2 o 4 Let the precursor solution stand for 24 hours, c...
Embodiment 2
[0046] Step 1, Co(NO 3 ) 2 ·6H 2 O and Fe(NO 3 ) 3 9H 2 O was dissolved in the mixture of ethylene glycol methyl ether and acetic anhydride, and stirred for 2 hours to obtain uniformly mixed CoFe 2 o 4 Precursor, CoFe 2 o 4 The concentration of Co ions in the precursor solution is 0.15mol / L, and the volume ratio of ethylene glycol methyl ether and acetic anhydride is 3:1;
[0047] Step 2, the Bi(NO 3 ) 3 ·5H 2 O, Tb(NO 3 ) 3 ·6H 2 O and Fe(NO 3 ) 3 9H 2 O is dissolved in a mixture of ethylene glycol methyl ether and acetic anhydride at a molar ratio of 0.94:0.11:1 (RE=Tb, x=0.11, 5% excess bismuth nitrate), and stirred for 2 hours to obtain a uniformly mixed Bi 0.89 Tb 0.11 FeO 3 Precursor, Bi 0.89 Tb 0.11 FeO 3 The total concentration of metal ions in the precursor solution is 0.3mol / L, and the volume ratio of ethylene glycol methyl ether and acetic anhydride is 3:1;
[0048] Step 3, the prepared CoFe 2 o 4 Let the precursor solution stand for 24 hour...
Embodiment 3
[0059] Step 1, Co(NO 3 ) 2 ·6H 2 O and Fe(NO 3 ) 3 9H 2 O was dissolved in the mixed solution of ethylene glycol methyl ether and acetic anhydride, stirred for 2 hours, and a uniformly mixed CoFe 2 o 4 Precursor, CoFe 2 o 4 The concentration of Co ions in the precursor solution is 0.2mol / L, and the volume ratio of ethylene glycol methyl ether and acetic anhydride is 3:1;
[0060] Step 2, the Bi(NO 3 ) 3 ·5H 2 O, Eu(NO 3 ) 3 ·6H 2 O and Fe(NO 3 ) 3 9H 2O is dissolved in a mixture of ethylene glycol methyl ether and acetic anhydride at a molar ratio of 0.95:0.1:1 (RE=Eu, x=0.1, excess bismuth nitrate), and stirred for 2 hours to obtain uniformly mixed Bi 0.9 Eu 0.1 FeO 3 Precursor, Bi 0.9 Eu 0.1 FeO 3 The total concentration of metal ions in the precursor solution is 0.3mol / L, and the volume ratio of ethylene glycol methyl ether and acetic anhydride is 3:1;
[0061] Step 3, the prepared CoFe 2 o 4 Let the precursor solution stand for 24 hours, clean the ...
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