Catalyst preparation system

A technology for preparing systems and catalysts, which can be used in catalyst activation/preparation, physical/chemical process catalysts, chemical instruments and methods, etc., and can solve the problems of batching, small processing capacity, and inability to produce non-uniform catalysts.

Inactive Publication Date: 2015-02-25
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, although these impregnation equipment can accomplish the purpose of impregnating the active material on the catalyst, there are many problems in these impregnation equipment and devices, such as intermittent operation, inability to realize continuous production, unstable product quality, and small processing capacity Shortcomings, catalyst support structure damage and other problems
[0004] In addition, many diffusion-limited catalytic reactions and highly exothermic catalytic reactions require heterogeneous catalysts to meet the requirements of the reaction process. Traditional production equipment can no longer meet the requirements of producing heterogeneous catalysts.

Method used

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Examples

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preparation example Construction

[0037] First, the present invention provides a catalyst preparation method, which is based on the impregnation method, that is, includes an impregnation step, and in the impregnation step, the purpose of impregnating the catalyst with an active component solution is achieved. The shape of the catalyst carrier has various shapes, such as circular, ellipsoid, Raschig ring and other structures. In addition, the active material in the active component solution mainly depends on the type of catalyst, such as various chemical elements such as alum and silver. In order to realize the purpose of the present invention, in the impregnation step of the preparation method provided by the invention, the catalyst carrier and the active component solution containing the active substance can be respectively input into the rotating drum 1 arranged at an inclination, and on the side of the rotating drum 1 The wall is provided with a turning member 11, wherein the active component solution is spr...

Embodiment 1

[0055]1. Put a strip-shaped alumina as a catalyst carrier and put it into the hopper-type carrier storage device 2, and enter the feed hopper 11 of the drum 1 through the second adjustment device 22 and the second conveyor belt 21 for transmission.

[0056] 2. The active component solution in the tank solution storage device 3 is transported through the pumping mechanism 32 first, and the active component in it is Ni+Mo, and then passes through the first regulating device 32 and enters the spray bar 5 and the atomizing nozzle 51 . The atomizing nozzle is a pressure nozzle, which can atomize the solution into droplets with a particle size of 20 microns to 120 microns, and spray them into the drum 1 at a volume flow rate of 0.3QM.

[0057] 3. Drive the rotating drum 1 by the rotating drive device 62, the rotating speed is 5 revolutions per minute, and the inner wall of the rotating drum 1 is provided with a material turning member 11, so that the catalyst carrier can be raised to...

Embodiment 2

[0061] 1. Put a strip-shaped alumina as a catalyst carrier and put it into the hopper-type carrier storage device 2, and enter the feed hopper 11 of the drum 1 through the second adjustment device 22 and the second conveyor belt 21 for transmission.

[0062] 2. The active component solution in the tank-type solution storage device 3 is first transported through the pumping mechanism 32 , and the active component therein is Co, then passes through the first regulating device 32 , and enters the spray bar 5 and the atomizing nozzle 51 . The atomizing nozzle is a pressure nozzle, which can atomize the solution into droplets with a particle size of 30 microns to 100 microns, and spray them into the drum 1 at a flow rate of 0.37 QM.

[0063] 3. Drive the rotating drum 1 by the rotating drive device 62, the rotating speed is 6 revolutions per minute, the inner wall of the rotating drum 1 is provided with a material turning member 11, so that the catalyst carrier can be raised to a ce...

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Abstract

The invention discloses a catalyst preparation system. The catalyst preparation system comprises a carrier storage device, a solution storage device and a rotary drum, wherein the carrier storage device is used for storing a catalyst carrier; the solution storage device is used for storing a solution containing active components; the rotary drum is inclined; the carrier storage device and the solution storage device are respectively communicated with the rotary drum; the solution containing the active components is sprayed into the rotary drum from the solution storage device in an atomizing form; a material turning piece is arranged on the side wall of the rotary drum and is used for turning the catalyst carrier which enters the rotary drum from the carrier storage device during the rotation of the rotary drum. According to the catalyst preparation system provided by the invention, the rotary drum which is used for impregnating the catalyst carrier can be inclined. Therefore, the catalyst carrier can move from the charge end to the discharge end when being impregnated by the solution containing the active components, so that a catalyst can be continuously prepared; moreover, by arranging the material turning piece on the side wall of the rotary drum, the catalyst carrier can be turned by the material turning piece during the rotation of the rotary drum, so that the effective contact effect of the catalyst carrier and active substances is improved.

Description

technical field [0001] The invention relates to the field of catalyst preparation, in particular to a catalyst preparation system. Background technique [0002] In the catalyst preparation and production process, there are many production methods, such as impregnation method, roll coating method, precipitation method, mixing method, ion exchange method, gas phase synthesis method and so on. Among them, the impregnation method is a more commonly used method. In the impregnation method, the impregnation step of impregnating the active component in the active component solution onto the catalyst support is the most important step. [0003] In the prior art, the traditional equipment for realizing the above impregnation steps can refer to the impregnation tanks, impregnation baskets, impregnation mesh belts, impregnation drums, impregnation drums, etc. Impregnation rolling ball machine, impregnation fluidized bed, etc. However, although these impregnation equipment can accomp...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J37/02
Inventor 侯朝鹏孙霞夏国富李明丰吴玉晋超阎振楠吴昊徐润聂红李大东
Owner CHINA PETROLEUM & CHEM CORP
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