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Impinging stream structure and impinging stream and rotary material packed bed device

A technology of rotating packed bed and impingement flow is applied in the field of strengthening liquid-liquid rapid micro-mixing reaction devices, which can solve the problems of unsatisfactory and uneven mixing effect of impinging flow structure, and achieve improved micro-mixing effect, reduction of by-products, and saving of by-products. cost effect

Active Publication Date: 2014-12-24
ZHONGBEI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In order to solve the problem of unsatisfactory and uneven mixing effect of the existing impingement flow structure, the present invention provides an impingement flow structure and an impingement flow-rotating packed bed device

Method used

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  • Impinging stream structure and impinging stream and rotary material packed bed device
  • Impinging stream structure and impinging stream and rotary material packed bed device
  • Impinging stream structure and impinging stream and rotary material packed bed device

Examples

Experimental program
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Effect test

Embodiment 1

[0031] A new impinging flow-rotating packed bed device is adopted 2 / d 1 =1.5, L 2 / d 2 =10,d 3 / D 1 =6, d 1 / D 1 =10,d 2 / D 1 =20. A, B solution volume flow ratio is 1, d 5 / d 4 =6. Research on diesel emulsification. 0.8000g / mL diesel oil is stored in the storage tank I7, which is solution A, and 3% emulsifier compounded by Tween80 and Span is placed in the storage tank II11, which is solution B, which passes through the pump and flow meter respectively ,, through the first impact of the impact flow in the cavity of the rotor, the formed mixed fluid enters the packing layer 2, and the rotor 3 rotates under the drive of the rotating shaft 6. When the speed is 1200r / min, the strong force generated by the supergravity field Centrifugal force makes the mixed fluid carry out secondary mixing and reaction, and finally enters the liquid outlet 5 and discharges, and the emulsified diesel oil is obtained without stratification for 1 month.

Embodiment 2

[0033] A new impinging flow-rotating packed bed device is adopted 2 / d 1 =10,L 2 / d 2 =30,d 3 / D 1 =1, d 1 / D 1 =100, d 2 / D 2 =2.5. A, B solution volume flow ratio is 5, d 5 / d 4 =2, research on paraffin emulsification. Solution A paraffin is placed in the liquid storage tank 7, and 5% of the emulsifier obtained by compounding Span80, K12 and co-emulsifier A is placed in the liquid storage tank 11, which is solution B. Corrosion pump II12, flowmeter I10, and flowmeter II14 are hit for the first time in the cavity of the hollow annular rotor through the new concussion flow, and the formed mixed fluid enters the packing layer 2, and the hollow annular rotor 3 is in the center of the rotating shaft 6. Driven to rotate, when the rotation speed is 1100r / min, the strong centrifugal force generated by the supergravity field makes the mixed fluid undergo secondary mixing and reaction, and finally enter the liquid outlet 5 and discharge, and the obtained paraffin emulsion ...

Embodiment 3

[0035] A new impinging flow-rotating packed bed device is adopted 2 / d 1 =20,L 2 / d 2 =50,d 3 / D 1 =10,d 1 / D 1 =50,d 2 / D 2 =100. A, B solution volume flow ratio is 20, d 5 / d 4 =2, for the preparation of microemulsion. Put 1mol / L HCl in the liquid storage tank I7, kerosene and 3% Span80 in the liquid storage tank II11, pass through the corrosion-resistant pump I8, corrosion-resistant pump II12, flowmeter I10, and flowmeter II14 respectively to adjust the solution The flow rate of A is 120L / h, and the flow rate of solution B is 80L / h. The passing and impinging flow makes the first impact in the cavity of the hollow annular rotor, and the formed mixed fluid enters the packing layer 2, and the hollow annular rotor 3 Driven by the rotating shaft 6, when the rotation speed is 900r / min, the strong centrifugal force generated by the supergravity field makes the mixed fluid undergo secondary mixing and reaction, and finally enter the liquid outlet 5 and discharge, and th...

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Abstract

The invention belongs to the technical field of devices for intensifying liquid and liquid quick micro mixing reaction, in particular relates to an impinging stream structure and an impinging stream and rotary material packed bed device, and solves the problem that the conventional impinging stream structure is not ideal and nonuniform in mixing effect. The impinging stream structure comprises a main feed pipe and a sleeve which are different in pipe diameter, wherein a plurality of main feed pipe discharge holes are formed in one side, near the sleeve, of the discharging section of the main feed pipe; the bottom of the sleeve corresponds to the discharging section of the main feed pipe; a plurality of sleeve discharge holes in one-one correspondence to the main feed pipe discharge holes in an up and down manner are coaxially formed in the bottom of the sleeve. According to the impinging stream and rotary material packed bed device, the impinging stream structure is arranged in a cavity of a rotor of the rotary material packed bed and is arranged in the axial direction of the rotor. the impinging stream structure and the impinging stream and rotary material packed bed have the advantages that fed feed in different amounts can be uniformly mixed, the reaction is quick, the reaction time is short, and the momentum loss is less, and are particularly suitable for quick reaction of batch feed feeding in different amounts in industry and the reaction system with the certain viscosity character.

Description

technical field [0001] The invention belongs to the technical field of enhanced liquid-liquid rapid microcosmic mixing reaction device, in particular to an impact flow structure and an impact flow-rotating packed bed device. Background technique [0002] Currently, impinging flow structures for liquid-liquid reactions are mainly submerged circulating impinging flow and impinging flow-rotating packed bed devices. However, there are still some deficiencies in the submerged circulating impingement flow. First of all, since the motor shaft on which the propeller is installed is a cantilever structure, if the shaft is longer or rotates faster, it is easy to cause vibration of the propeller and the motor shaft. Secondly, the motor shaft on which the propeller is installed needs to be installed with a shaft seal structure on the reactor wall, which increases the manufacturing cost of the reactor, and the shaft seal structure is easily damaged during long-term operation, which aff...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J4/00B01J19/26B01J14/00
Inventor 刘有智焦纬洲祁贵生张珺袁志国栗秀萍申红艳高璟张巧玲罗莹
Owner ZHONGBEI UNIV
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