Equipment and method for removing light components through inert gas circulation gas stripping

A technology of inert gas and light components, applied in chemical instruments and methods, preparation of organic compounds, preparation of carboxylic acid esters, etc., can solve the problems of high cost, poor separation effect, and unsuitable for large-scale production and use. , to achieve the effect of preventing reaction, reducing the probability of reaction and avoiding blockage

Active Publication Date: 2014-12-10
TIANJIN AOZHAN XINGDA TECH
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Problems solved by technology

In order to reduce the heating temperature of heat-sensitive materials and prevent heat-sensitive materials from decomposing or polymerizing and deteriorating at high temperatures, there are many studies on the separation and purification of heat-sensitive materials at home and abroad, and there are many separation methods, such as vacuum distillation, molecular distillation, and chromatographic separation. and other methods, but the separation effect is not good, and the cost is high, most of the methods are not suitable for industrial large-scale production and use

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  • Equipment and method for removing light components through inert gas circulation gas stripping

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Embodiment Construction

[0022] Such as figure 1 As shown, an inert gas circulating stripping device for removing light components of the present invention includes: a stripping tower 3, a light component collection tank 6, a heavy component collection tank 11, a demister 8, and a first heater 1 , the second heater 2, the first cooling device 4, the second cooling device 10, the ultra-low temperature condenser 5, the circulating fan 9 and the vacuum pump 7; the stripper 3 upper side wall is respectively provided with a feed inlet 13 and an air outlet 15 , the side wall of the middle and lower part is provided with an air inlet 14, and the bottom is provided with a heavy component outlet 18; the air inlet 14 of the stripper 3 communicates with the inert gas delivery pipe 17; the inert gas delivery pipe 17 is provided with a regulating valve 12 and The first heater 1; the feed port 13 of the stripper 3 communicates with the material delivery pipe 16; the material delivery pipe 16 is provided with the se...

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Abstract

The invention discloses equipment and method for removing light components through inert gas circulation gas stripping and relates to equipment and method which utilize gas stripping and steam condensation. The invention aims to provide equipment and method for removing light components through inert gas circulation gas stripping with the advantages of low cost and applicability to heat-sensitive materials. The equipment disclosed by the invention comprises a gas stripping tower, a light component collection tank, a heavy component collection tank, a demister, a first heater, a second heater, a first cooling device, a second cooling device, an ultralow temperature condenser, a circulating fan and a vacuum pump. The method disclosed by the invention comprises the following steps: heating inert gases; heating materials; carrying out gas stripping; cooling and collecting the light components and heavy components and recycling the inert gases. According to the equipment and method disclosed by the invention, local heating of the materials can be reduced, coking is avoided, and the reaction among the heat-sensitive materials is avoided; and moreover, the equipment can operate continuously and is suitable for large-scale industrial production. The equipment and method disclosed by the invention are applied to the separation field of organic matter monomers and intermediates, fine chemical engineering products, medicines, spices and the like.

Description

technical field [0001] The present invention relates to a kind of equipment and method utilizing gas stripping and condensation of steam, especially relates to a kind of equipment and method of heat-sensitive material separation. Background technique [0002] Heat-sensitive materials widely exist in industrial production and daily life. They are unstable to temperature. They will coke, carbonize and be easily oxidized when heated for a long time. This property brings great difficulty to the separation of heat-sensitive materials. In industrial production and daily life, we often encounter heat-sensitive substances, such as many organic monomers and intermediates, fine chemical products, medicines, spices, etc. In order to reduce the heating temperature of heat-sensitive materials and prevent heat-sensitive materials from decomposing or polymerizing and deteriorating at high temperatures, there are many studies on the separation and purification of heat-sensitive materials at...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D3/38C07C69/30C07C67/54C07C69/533C07C69/58C07C69/587
Inventor 李建明阮杰张春璐
Owner TIANJIN AOZHAN XINGDA TECH
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