Polypyrrole-polyaniline/Fe3O4 compound and preparation method thereof
A composite and aniline technology, applied in the direction of ferrous oxide, iron oxide/iron hydroxide, etc., can solve the problems of uneven dispersion and complexity of magnetic particles
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Embodiment 1
[0076] Embodiment 1: poly(pyrrole-aniline) / Fe of the present invention 3 o 4 Preparation of complex
[0077] The implementation steps of this embodiment are as follows:
[0078] A. Preparation of white emulsion
[0079] Add 6.5mmol of pyrrole to 80ml of ammonia solution with a concentration of 1.4mol / L, and use an ultrasonic device sold under the trade name Ultrasonic Cleaner by Gowell Technology Co., Ltd. to ultrasonically treat the resulting mixture at a frequency of 20KHz and a power of 80w 2min, obtain a kind of white emulsion;
[0080] B. Add ferrous chloride
[0081] At a temperature of 20°C, according to FeCl 2 4H 2 The molar ratio of O to pyrrole is 1:2.4, add 0.5mol / LFeCl to the white emulsion obtained in step A 2 4H 2 O aqueous solution, obtains the solution containing ferrous chloride;
[0082] C. Add ferric chloride
[0083] According to FeCl 2 .4H 2 O and FeCl 3 ·6H 2 The molar ratio of O is 1:50, add 6.0mol / LFeCl dropwise to the ferrous chloride sol...
Embodiment 2
[0093] Embodiment 2: poly(pyrrole-aniline) / Fe of the present invention 3 o 4 Preparation of complex
[0094] The implementation steps of this embodiment are as follows:
[0095] A. Preparation of white emulsion
[0096] Add 1.0mmol of pyrrole to 100ml of ammonia solution with a concentration of 1.0mol / L, and use ultrasonic equipment sold by Gowell Technology Co., Ltd. under the trade name Ultrasonic Cleaner, and ultrasonically treat the resulting mixture at a frequency of 30KHz and a power of 80w. 2min, obtain a kind of white emulsion;
[0097] B. Add ferrous chloride
[0098] At a temperature of 5°C, according to FeCl 2 4H 2 The molar ratio of O to pyrrole is 1:0.3, add 0.3mol / LFeCl to the white emulsion obtained in step A 2 4H 2 O aqueous solution, obtains the solution containing ferrous chloride;
[0099] C. Add ferric chloride
[0100] According to FeCl 2 .4H 2 O and FeCl 3 ·6H 2 The molar ratio of O is 1:31, add 3.0mol / LFeCl dropwise to the ferrous chloride ...
Embodiment 3
[0106] Embodiment 3: Poly(pyrrole-aniline) / Fe of the present invention 3 o 4 Preparation of complex
[0107] The implementation steps of this embodiment are as follows:
[0108] A. Preparation of white emulsion
[0109] Add 3.8mmol pyrrole to the 90ml ammonia solution with a concentration of 1.2mol / L, and use the ultrasonic equipment sold by Gowell Technology Co., Ltd. under the trade name Ultrasonic Cleaner, and ultrasonically treat the obtained mixture under the condition of frequency 20KHz and power 120w 4min, obtain a kind of white emulsion;
[0110] B. Add ferrous chloride
[0111] At a temperature of 25°C, according to FeCl 2 4H 2 The molar ratio of O to pyrrole is 1:3.0, add 0.3mol / LFeCl to the white emulsion obtained in step A 2 4H 2 O aqueous solution, obtains the solution containing ferrous chloride;
[0112] C. Add ferric chloride
[0113] According to FeCl 2 .4H 2 O and FeCl 3 ·6H 2 The molar ratio of O is 1:78, add 4.0mol / LFeCl dropwise to the ferrou...
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