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Preparation method of Sm-Co alloy amorphous magnetic nanowire array

A magnetic nanometer and wire array technology, applied in nanotechnology and other fields, can solve the problem of low deposition rate of Sm-Co alloy nanowires, and achieve the effects of good repeatability, simple process, and strong controllability of process technical parameters

Active Publication Date: 2014-10-08
HEBEI UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, in the existing techniques for electrodeposition of rare earth alloys in aqueous solution, the deposition rate of Sm-Co alloy nanowires obtained is very low

Method used

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  • Preparation method of Sm-Co alloy amorphous magnetic nanowire array
  • Preparation method of Sm-Co alloy amorphous magnetic nanowire array
  • Preparation method of Sm-Co alloy amorphous magnetic nanowire array

Examples

Experimental program
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Embodiment 1

[0039] The first step is to install a dedicated Sm-Co alloy amorphous nanowire deposition device:

[0040] The installation of the dedicated Sm-Co alloy amorphous nanowire deposition device used in this embodiment is as follows: figure 1 In the illustrated embodiment, the raw material used in the AAO template 4 is aluminum foil with a purity of 99.999%, its thickness is 12 microns, the aperture size is 60 nanometers, and the graphite C electrode 1 is a graphite plate with a size of 8 cm × 5 cm × 2 cm;

[0041] The second step is the pretreatment of the AAO template and the preparation of the electrolytic deposition solution:

[0042] First soak the AAO template 4 in deionized water, place it in a 60°C water bath for 1 min, then place it in an ultrasonic generator and vibrate with ultrasonic waves until the air bubbles in the nanopores are fully driven away, and prepare for use. Chemical reagent SmCl 3 ·6H 2 O, CoCl 2 ·6H 2 O, H 3 BO 3 , glycine and ascorbic acid are dis...

Embodiment 2

[0049] The first step is to install a dedicated Sm-Co alloy amorphous nanowire deposition device:

[0050] The installation of the dedicated Sm-Co alloy amorphous nanowire deposition device used in this embodiment is as follows: figure 1 In the illustrated embodiment, the raw material used in the AAO template 4 is aluminum foil with a purity of 99.999%, its thickness is 12 microns, the aperture size is 60 nanometers, and the graphite C electrode 1 is a graphite plate with a size of 8 cm × 5 cm × 2 cm;

[0051] The second step is the pretreatment of the AAO template and the preparation of the electrolytic deposition solution:

[0052] First, soak the AAO template 4 in deionized water, place it in a 60°C water bath for 1 min, and then place it in an ultrasonic wave to fully drive away the air bubbles in the nanopores. 3 ·6H 2 O, CoCl 2 ·6H 2 O, H 3 BO 3 , glycine and ascorbic acid are dissolved and prepared to obtain electrolytic deposition solution 2, and the molar concen...

Embodiment 3

[0059] The first step is to install a dedicated Sm-Co alloy amorphous nanowire deposition device:

[0060] The installation of the dedicated Sm-Co alloy amorphous nanowire deposition device used in this embodiment is as follows: figure 1 In the illustrated embodiment, the raw material used in the AAO template 4 is aluminum foil with a purity of 99.999%, its thickness is 12 microns, the aperture size is 60 nanometers, and the graphite C electrode 1 is a graphite plate with a size of 8 cm × 5 cm × 2 cm;

[0061] The second step is the pretreatment of the AAO template and the preparation of the electrolytic deposition solution:

[0062] First, soak the AAO template 4 in deionized water, place it in a 60°C water bath for 1 min, and then place it in an ultrasonic wave to fully drive away the air bubbles in the nanopores. 3 ·6H 2 O, CoCl 2 ·6H 2 O, H 3 BO 3 , glycine and ascorbic acid are dissolved and prepared to obtain electrolytic deposition solution 2, and the molar concen...

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Abstract

The invention discloses a technical scheme of a preparation method of a Sm-Co alloy amorphous magnetic nanowire array, relates to amorphous alloy of which the main component is cobalt. The preparation method comprises the following steps: performing nanowire deposition in electrolytic deposition liquid which is prepared by using 100mL of de-ionized water and has a molar concentration ratio of SmCl3.6H2O to CoCl2.6H2O to H3BO3 to glycine to ascorbic acid being (0.5-1.8) to (2-5) to (5-10) to (4-8) to (3-7) in an electrolytic deposition tank of a special Sm-Co alloy amorphous magnetic nanowire deposition device, and annealing the deposited Sm-Co alloy amorphous magnetic nanowire array to prepare a Sm-Co alloy amorphous magnetic nanowire array product. According to the method, the defect of low deposition rate of Sm-Co alloy nanowires, namely the Sm-Co alloy amorphous magnetic nanowire array in the prior art is overcome.

Description

technical field [0001] The technical scheme of the invention relates to an amorphous alloy with samarium cobalt as the main component, specifically a method for preparing an Sm-Co alloy amorphous magnetic nanowire array. Background technique [0002] Sm–Co alloys have better magnetic properties than transition metals and their alloys. As the most viable new nano-magnetic materials, new application growth points for Sm–Co industry are constantly emerging. In addition to high-density magnetic storage media, magnetic In addition to being widely used in the fields of fluids, household appliances and biomedicine, it has also greatly promoted the potential development of micro-devices in the computer, information and electromechanical industries. Therefore, people began to study the Sm-Co nano-magnetic materials. Since 1982, Hu Zuoqi, Zhang Yulong and others have conducted creative research on amorphous Sm–Co perpendicular magnetization films, and found that Sm–Co alloys have hig...

Claims

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Application Information

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IPC IPC(8): C25C5/02C25D3/56C25D5/50B82Y40/00
Inventor 崔春翔杨薇刘巧稚曹斌
Owner HEBEI UNIV OF TECH
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