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Microwave-assisted preparation method of bagasse bleached pulp

A bagasse and microwave technology, which is used in pulping of cellulose raw materials, textiles and papermaking, papermaking, etc., can solve problems such as unreported, and achieve the effects of simple operation, high whiteness and low kappa value.

Inactive Publication Date: 2014-08-27
KUNMING UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But unfortunately, the use of microwaves for pulping and bleaching is still carried out according to the traditional multi-step process. For example, plant raw materials are chemically pulped by microwaves to obtain natural color pulp [7] ; In the microwave bleaching process, it is often to improve the technology of a certain bleaching process, and the bleaching object is mostly the natural color paste of a certain plant [8-10] , and the technology of directly preparing bleached pulp by using microwave heating technology with plant raw materials as the research object has not been reported yet.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Example 1: The microwave preparation method of bagasse bleached pulp, concrete operation is as follows:

[0033] (1) Microwave water extraction process of bagasse raw material

[0034] The bagasse raw material is air-dried, wherein the moisture of the air-dried raw material varies according to the air humidity in different regions and seasons, and is generally controlled within the range of 5-20%;

[0035] The water extraction treatment conditions are: add deionized water according to the ratio of 1g of absolute dry bagasse raw material to 50ml of deionized water, microwave power 200w, action time 60min.

[0036] The specific processing steps are: mix 15g of absolutely dry bagasse raw material (if the moisture content of the air-dried raw material is 5.00%, weigh 15.8g of air-dried bagasse) and 750ml of deionized water in a microwave heating polypropylene fresh-keeping box, mix them evenly, and put them into the microwave reaction Under the power of 200w, the water is...

Embodiment 2

[0046] Example 2: The microwave preparation method of bagasse bleached pulp, concrete operation is as follows:

[0047] (1) Microwave water extraction process of bagasse raw material

[0048] The bagasse raw material is air-dried, wherein the moisture of the air-dried raw material varies according to the air humidity in different regions and seasons, and is generally controlled within the range of 5-20%;

[0049] The water extraction treatment conditions are as follows: add deionized water according to the ratio of 100ml deionized water to 1g absolute dry bagasse raw material, microwave power 400w, action time 35min.

[0050] The specific processing steps are: fully mix 15g of absolute dry bagasse raw material (if the moisture content of the air-dried raw material is 10.00%, then weigh 16.7g of air-dried bagasse) and 1500ml of deionized water in a polypropylene fresh-keeping box for microwave heating, and put it into the microwave reaction Under the power of 400w, the water...

Embodiment 3

[0060] Embodiment 3: The microwave preparation method of bagasse bleached pulp, concrete operation is as follows:

[0061] (1) Microwave water extraction process of bagasse raw material

[0062] The bagasse raw material is air-dried, wherein the moisture of the air-dried raw material varies according to the air humidity in different regions and seasons, and is generally controlled within the range of 5-20%;

[0063] The water extraction treatment conditions are: add deionized water according to the ratio of 1g of absolute dry bagasse raw material to 200ml of deionized water, microwave power 800w, action time 15min.

[0064] The specific processing steps are: fully mix 15g of absolutely dried bagasse raw material (if the moisture content of the air-dried raw material is 20.00%, then weigh 18.8g of air-dried bagasse) and 3000ml of deionized water in a polypropylene fresh-keeping box for microwave heating, and put it into the microwave reaction Under the power of 800w in the dev...

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PUM

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Abstract

The invention discloses a microwave-assisted preparation method of bagasse bleached pulp, which is a method for clean and high-efficient preparation of bagasse bleached pulp by microwave radiation technology. The method comprises: performing microwave heating and water extracting treatment of air-dried bagasse raw materials, repeatedly soaking and cleaning the treated materials with deionized water to be neutral, then performing dehydration and dispersion, rapidly determining the water content of the dispersed materials, then performing delignification treatment of the materials with a known water content by sodium hydroxide / hydrogen peroxide / anthraquinone, finally soaking, dispersing and washing the treated pulp to be neutral, removing excessive water, and sealing to obtain the bagasse bleached pulp. The bagasse bleached pulp prepared by the method is milk white or in a white fiber form, low in paper pulp kappa number, high in whiteness, and moderate in viscosity.

Description

technical field [0001] The invention relates to a method for cleanly and efficiently preparing bleached pulp by using bagasse, a solid waste after sugar extraction, as a raw material, and belongs to the technical field of pulp and papermaking. Background technique [0002] With the rapid development of the pulp and paper industry, the supply of wood fiber raw materials is increasingly in short supply. In addition to vigorously developing "forest-paper integration", making full use of non-wood raw materials is an important way to develop the paper industry. Bagasse is the solid residue of fibrous cells and miscellaneous cells (mostly parenchyma cells) left after sugar cane is squeezed, referred to as bagasse. Yunnan, the second largest sugar-producing province in China, produces about 1.7 million tons of bagasse a year [1] . According to the literature records, due to the suitable aspect ratio of bagasse fibers after removing pith, the similar pulping properties to wood pul...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D21C3/22
Inventor 张恒高欣陈克利陈海燕朱正良
Owner KUNMING UNIV OF SCI & TECH
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