Chemically stable low-oil-adhesiveness oil-water separating member, and making method and use thereof
A low oil adhesion, oil-water separation membrane technology, applied in separation methods, chemical instruments and methods, liquid separation, etc. Contamination and other problems, to achieve fast and efficient separation performance, strong anti-swelling and corrosion, low cost effect
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[0042] More specifically, the preparation method of the present invention includes: taking the aforementioned substrate precursor as the substrate, adopting a method of etching in a high-concentration alkaline solution, and adjusting the temperature of the reaction system and the oxidation time, so that on the aforementioned substrate precursor, For example, an oil-water separation membrane with an inorganic nanosheet structure of a metal oxide or hydroxide with a rough micro / nano structure surface is prepared on a metal grid or a foam material support.
[0043] In a typical embodiment, the preparation method of the oil-water separation membrane comprises:
[0044] A substrate precursor with a plurality of through holes is provided, wherein at least the surface layer of the substrate precursor and the walls of the through holes are covered with a material layer mainly composed of iron, and the diameter of the through holes is 100-2000 head,
[0045] taking the substrate precu...
Embodiment 1
[0059] (1) The 250-mesh stainless steel mesh was immersed in deionized water and ethanol for ultrasonic cleaning, then washed with deionized water and dried naturally.
[0060] (2) At room temperature, add 100mL of water, 3g of sodium hydroxide and 0.96g of potassium persulfate into a 150mL beaker, mix evenly with magnetic stirring, prepare a uniform aqueous solution, and raise the temperature to 70°C for later use.
[0061] (3) Soak the pre-cleaned stainless steel in step (1) in the solution to react, and the reaction time is 3 hours, thereby forming iron oxide nanosheets coated with metal mesh on the surface of the metal mesh, the height of the nanosheet is about 100 Nano, width is about 100 nanometers, take out the omentum after the reaction is completed, wash it repeatedly with deionized water, and dry it naturally in the air to obtain super hydrophilic in the air environment and underwater and super hydrophilic in the underwater Oleophobic oil-water separation membrane, t...
Embodiment 2
[0066] (1) The 500-mesh stainless steel mesh was immersed in deionized water and ethanol for ultrasonic cleaning, then washed with deionized water and dried naturally.
[0067] (2) At room temperature, add 100mL of water, 2.7g of potassium hydroxide and 4.32g of ammonium persulfate into a 150mL beaker, stir evenly with magnetic force, prepare a uniform aqueous solution, and raise the temperature to 50°C for later use.
[0068] (3) Soak the pre-cleaned stainless steel mesh in step (1) in the solution to react. The reaction time is 6 hours, thereby forming iron oxide nanosheets coated with metal mesh on the surface of the metal mesh. The height of the nanosheets is about 300 nanometers and a width of about 300 nanometers. The omentum after the reaction is taken out, washed repeatedly with deionized water, and dried naturally in the air. An oil-water separation membrane with superoleophobic properties, the membrane has a pore size of about 10-20 microns, and its surface appearanc...
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