Method for preparing high dielectric polymer composite film
A technology of dielectric polymer and composite film, applied in chemical instruments and methods, synthetic resin layered products, layered products, etc., to achieve the effect of good application prospects
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example 1
[0059] ①Dissolve polyvinylidene fluoride in N, N dimethylformamide solvent, the concentration of polyvinylidene fluoride is 1 mol / liter, to form a polyvinylidene fluoride solution for LB film preparation;
[0060] ② Use a micro-sampler to extract 400 μl of the polyvinylidene fluoride solution obtained in ①, and add it to the surface of the ultrapure water in the LB membrane tank, and the polyvinylidene fluoride spreads on the gas / liquid interface and forms an ordered film;
[0061] ③Control the sliding barrier of the LB film equipment to compress the polyvinylidene fluoride film at a speed of 0.5 mm / min to a film pressure of 15 mN / m, and transfer the polyvinylidene fluoride film to the aluminum substrate by vertical film formation. The film formation rate is 0.1 mm / min;
[0062] 4. Barium titanate nanoparticles and ferric chloride are dissolved in n-butanol / ultrapure aqueous solution, the concentration of barium titanate nanoparticles is 30 mg / ml, and the concentration of ferr...
example 2
[0069] In Example 2, the polymer is polyimide, and the rest of the materials and manufacturing process are similar to those in Embodiment 1, thereby obtaining polyimide / polythiophene / barium titanate nanoparticles / polyimide high-dielectric composite film.
example 3
[0071] In Example 3, the polymer is polystyrene, and the rest of the materials and manufacturing process are similar to those in Embodiment 1, so as to obtain polystyrene / polythiophene / barium titanate nanoparticles / polystyrene high-dielectric composite film.
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