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Preparation method of light-weight silica brick

A silica brick, lightweight technology, applied in the field of refractory materials, can solve problems such as uneven distribution, low porosity, and affecting the stability of lightweight materials, and achieve the goal of reducing bulk density, reducing thermal conductivity, and improving the degree of uniform distribution Effect

Inactive Publication Date: 2014-06-25
WUHAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there is an obvious shortcoming in the machine-compressed combustible method, that is, there is a problem of uneven distribution of raw materials in the process of mixing and machine-pressing, especially in which combustibles are difficult to mix evenly in dry mixing, and there is often particle segregation, resulting in After the material is fired, the microstructure is uneven, for example: some parts have high porosity, and some parts have low porosity; which in turn affects the stability of light material properties, such as high temperature volume stability, load softening temperature and thermal conductivity, etc.
[0006] Furthermore, iron scale and lime milk are widely used as mineralizers in the production of traditional lightweight silica bricks, both of which will reduce the high-temperature mechanical properties of the material; With suitable strength, lignin sulfonate is often added as a binder when mixing raw materials, which will also reduce the high temperature mechanical properties of the product

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A method for preparing lightweight silica bricks. First mix 30~40wt% of silica particles, 20~30wt% of silica fine powder, 2~4wt% of limestone, 10~15wt% of silica sol and 20~30wt% of coke, stir evenly, and vibrate to form; The molded green body is dried at 110°C for 4-8 hours, and then kept at 1200-1300°C for 3-7 hours to obtain lightweight silica bricks.

Embodiment 2

[0029] A method for preparing lightweight silica bricks. First mix 40~50wt% of silica particles, 10~20wt% of silica fine powder, 4~6wt% of limestone, 10~15wt% of silica sol and 10~20wt% of coke, stir evenly, and pound into shape; Dry the molded green body at 110°C for 8-15 hours, and then keep it at 1300-1400°C for 7-10 hours to obtain lightweight silica bricks.

Embodiment 3

[0031] A method for preparing lightweight silica bricks. First mix 50~60wt% of silica particles, 10~20wt% of silica fine powder, 4~6wt% of limestone, 5~10wt% of silica sol and 10~20wt% of coke, stir evenly, and vibrate to form; The molded green body is dried at 110°C for 15-20 hours, and then kept at 1300-1400°C for 10-12 hours to obtain lightweight silica bricks.

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Abstract

The invention relates to a preparation method of a light-weight silica brick. According to the technical scheme, the preparation method comprises the following steps: uniformly mixing 30wt%-60wt% of silica particles, 10wt%-30wt% of fine silica powder, 2wt%-6wt% of limestone, 5wt%-15wt% of silica sol and 10wt%-30wt% of coke, and vibrating or ramming for forming; and drying formed blank bodies at 110 DEG C for 4-24 hours, and insulating at 1200-1400 DEG C for 3-15 hours to obtain the light-weight silica brick. The preparation method is simple in process, the adopted raw materials are rich, and the prepared light-weight silica brick has the characteristics of uniform microscopic structures, small volume density, excellent heat insulation performance, high refractoriness under load, good high-temperature volume stability, rich raw materials and wide application range.

Description

technical field [0001] The invention belongs to the technical field of refractory materials. In particular, it relates to a method for preparing lightweight silica bricks. Background technique [0002] With the increasing shortage of energy, countries pay more and more attention to the development, production and use of energy-saving materials for high-temperature industry. Due to the characteristics of light weight, high porosity, low bulk density and low thermal conductivity, lightweight refractory materials have obvious advantages in energy saving, so they have been widely used in high-temperature industries, playing the role of heat preservation, energy saving and consumption reduction. [0003] Silica bricks have been widely used and researched in lightweight refractory systems due to their high load softening temperature, good volume stability at high temperatures, and no shrinkage after long-term use. At present, there are many methods for manufacturing lightweight ...

Claims

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Application Information

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IPC IPC(8): C04B35/66C04B38/06
Inventor 魏耀武李楠
Owner WUHAN UNIV OF SCI & TECH
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