Carboxymethyl starch sizing agent and preparation method thereof
A carboxymethyl starch and sizing agent technology, which is applied in the direction of water repellent addition, inorganic compound addition, paper, etc., can solve the problems of poor low temperature stability of sizing agents, lower paper quality, low surface strength, etc., and achieve good low temperature Stabilization, strength-enhancing effects
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Embodiment 1
[0012] A kind of preparation method of carboxymethyl starch sizing agent, preparation method comprises the following steps: (1) take carboxymethyl starch at room temperature to be 9kg, drop into reaction kettle, then add castor oil phosphate to be 7kg, deionized water to be 185kg, mechanical stirring, the stirring speed is 150rpm, stirring until the solution is fully emulsified and uniform; (2) Add 5 kg of polyethylene glycol, 3 kg of gelatin, 7 kg of methyl propylene glycol, and 4 kg of potassium carbonate into the reaction kettle, and carry out mechanical stirring again. Stirring, the stirring speed is 150rpm, and the time is 15min; (3) The mixed liquid in the reaction kettle is sheared with a high-speed shearing machine, the shearing speed is 3000rpm, and the shearing time is 20min; The temperature of the glue is lowered to room temperature and stored.
Embodiment 2
[0014] A kind of preparation method of carboxymethyl starch sizing agent, preparation method comprises the following steps: (1) get carboxymethyl starch at room temperature to be 11kg, put into reaction kettle, then add castor oil phosphate to be 8kg, deionized water is 190kg, mechanical stirring, the stirring speed is 150rpm, stirring until the solution is fully emulsified and uniform; (2) Add 4 kg of polyethylene glycol, 4 kg of gelatin, 7 kg of methyl propylene glycol, and 2 kg of potassium carbonate into the reaction kettle, and carry out mechanical stirring again. Stirring, the stirring speed is 150rpm, and the time is 15min; (3) The mixed liquid in the reaction kettle is sheared with a high-speed shearing machine, the shearing speed is 3500rpm, and the shearing time is 20min; The temperature of the glue is lowered to room temperature and stored.
Embodiment 3
[0016] A kind of preparation method of carboxymethyl starch sizing agent, preparation method comprises the following steps: (1) take carboxymethyl starch at room temperature to be 10kg, put into reaction kettle, then add castor oil phosphate to be 6kg, deionized water is 187kg, mechanical stirring, the stirring speed is 150rpm, stirring until the solution is fully emulsified and uniform; (2) Add 5 kg of polyethylene glycol, 6 kg of gelatin, 8 kg of methyl propylene glycol, and 3 kg of potassium carbonate into the reaction kettle, and carry out mechanical stirring again. Stirring, the stirring speed is 150rpm, and the time is 15min; (3) The mixed liquid in the reaction kettle is sheared with a high-speed shearing machine, the shearing speed is 4000rpm, and the shearing time is 20min; (4) After the shearing, it is to be applied The temperature of the glue is lowered to room temperature and stored.
[0017] The carboxymethyl starch sizing agents of Example 1, Example 2, and Examp...
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