Preparation method of jujube subcritical extract and application of jujube subcritical extract in cigarette
An extraction method and extract technology, which are applied in the field of preparation of jujube extract, can solve the problems of affecting products, restricting application, and high temperature, and achieve the effects of improving taste, improving the quality of absorbing food, and improving the quality of absorbing food.
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Embodiment 1
[0020] a. Put the jujube, which has been washed, removed impurities, and pitted, in an oven at 60°C for 24 hours, and then pulverize it twice with a traditional Chinese medicine grinder to 40 mesh;
[0021] B, get the jujube powder material that step a gained, carry out dimethyl ether subcritical critical extraction under the following conditions: extraction pressure 0.61Mpa, extraction temperature 25 ℃; With 95% ethanol as entrainer, ethanol consumption is jujube powder 3 times of the material (weight ratio). Extraction time 1.5h;
[0022] c. After the extraction is finished, the extraction mixture enters the separation tank, and the extraction solvent is separated by the principle of vacuum evaporation to obtain the jujube subcritical extract.
[0023] After the jujube extract is dissolved in 95% ethanol solution, it is added to the shredded tobacco in the feeding process by spraying, and the dosage of the jujube extract is 0.05% of the mass of the shredded tobacco.
[002...
Embodiment 2
[0026] a. The jujubes that have been washed, removed impurities, air-dried and pitted are placed in an oven at 70°C and dried for 24 hours, and then pulverized twice with a traditional Chinese medicine pulverizer to 50 mesh;
[0027] b. Take the jujube powder obtained in step a, and carry out butane subcritical extraction under the following conditions: extraction pressure 0.34Mpa, extraction temperature 35°C; 70% ethanol as entrainer, ethanol consumption is jujube powder 2 times (weight ratio). Using dimethyl ether subcritical extraction method to extract jujube powder for 1.0h;
[0028] c. After the extraction is finished, the extraction mixture enters the separation tank, and the extraction solvent is separated by the principle of vacuum evaporation to obtain the jujube subcritical extract.
[0029] After dissolving the above-mentioned jujube extract in 95% ethanol solution, it is added to the shredded tobacco in the feeding process by spraying, and the dosage of the jujub...
Embodiment 3
[0032] a. Put the jujube, which has been washed, removed impurities, and pitted, in an oven at 80°C for 24 hours, and then pulverize it twice with a traditional Chinese medicine grinder to 60 mesh;
[0033] B, get the jujube powder material that step a gained, carry out propane subcritical critical extraction under the following conditions: extraction pressure 0.45Mpa, extraction temperature 45 ℃; With 95% ethanol as entrainer, ethanol consumption is the jujube powder material 5 times (weight ratio). The jujube powder was extracted by dimethyl ether subcritical extraction method for 0.5h;
[0034] c. The extraction mixture enters the evaporation system after solid-liquid separation, and under the action of a compressor and a vacuum pump, the extraction agent is converted from a liquid state to a gas state according to the principle of reduced-pressure evaporation, thereby obtaining the jujube extract.
[0035] After dissolving the above-mentioned jujube extract in 95% ethanol...
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