Eucommia ulmoides key fruit hull treating method beneficial to extraction of gutta-percha

A technology of Eucommia samara and treatment method, which is applied in the field of treatment of Eucommia samara shell, can solve the problems of long extraction time, poor penetration, and environmental pollution, and achieve excellent treatment effect, improved penetration, and excellent environmental benefits Effect

Inactive Publication Date: 2014-04-30
JISHOU UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In order to obtain eucommia gum with high purity, it is generally extracted with non-polar organic solvents such as petroleum ether and then analyzed, but the penetration of non-polar solvents to hydrophilic substances such as cellulose, pectin and lignin is relatively low. Poor, the gum filaments in the Eucommia husk are wrapped and densely covered by plant cell tissues with cellulose, pectin and lignin as the main components, so there is a large transmission in the extraction process with non-polar solvents such as petroleum ether. Material resistance, the solvent is difficult to pass through the plant cell tissue to dissolve the Eucommia gum, and the solution dissolved in the Eucommia gum is also difficult to release, the extraction time is long and the efficiency is low, and there are still more Eucommia gum left in the shell after the gel is extracted
[0004] In order to reduce the mass transfer resistance, most of the existing technologies use enzymatic hydrolysis, biological fermentation or alkaline solution to pretreat the raw materials, and use enzyme preparations or alkaline solutions to erode the cell tissues of Eucommia ulmoides such as cellulose, pectin and lignin to enhance Solvent penetration, but enzymatic hydrolysis has the problems of long time, high cost and poor effect. Alkali treatment will produce a large amount of waste liquid, which seriously pollutes the environment; among many methods, biological fermentation is an ideal method, but Most of the current biological fermentations use koji and yeast for fermentation, which takes a long time and has poor effects. Therefore, it is necessary to screen strains with strong specificity and good treatment effects and develop the technology for treating Eucommia samara shells

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] (1) Preparation of the seed liquid of the white rot fungus: Inoculate the white rot bacteria of the white rot fungus on a newly prepared PDA plate with a diameter of 9 cm, activate the mycelia for 4 days to cover the plate, and inoculate one plate of fungus The silk was inoculated into a shaker flask equipped with 400 mL of PDA liquid medium, and cultured on a shaker at 27° C. for 76 hours to obtain a seed liquid of R. albicans.

[0015] (2) Inoculation and cultivation of samara shell of Eucommia ulmoides: Soak samara shell of Eucommia ulmoides in water for 15 hours and make the water content of the shell 65%. The inoculated fruit shells are piled up for fermentation, and the ambient temperature is kept at 27°C and the humidity is 82% to ferment for 14 days. During the fermentation period, the fungus albicans occurs, and the shell material is filled with white hyphae until the mycelium slowly dissolves.

[0016] (3) Treatment after fermentation: After the fermentation i...

Embodiment 2

[0019] (1) Preparation of the seed solution of the white rot fungus: Inoculate the white rot bacteria of the white rot fungus on a newly prepared PDA plate with a diameter of 9 cm, activate the mycelia for 5 days to cover the plate, and inoculate one plate of bacteria The silk was inoculated into a shaker flask equipped with 400 mL of PDA liquid medium, and cultured on a shaker at 28° C. for 62 hours to obtain a seed liquid of R. albicans.

[0020] (2) Inoculation and cultivation of samara shell of Eucommia ulmoides: Soak samara shell of Eucommia ulmoides in water for 11 hours and make the water content of the samara 73%, inoculate the seed liquid of eucommia samara according to 0.99% of the mass of samara eucommia husk, and The inoculated husks were piled up for fermentation, and kept at an ambient temperature of 29°C and a humidity of 90% for 11 days of fermentation. During the fermentation period, the fungus albicans occurred, and the husk material was filled with white myce...

Embodiment 3

[0024] (1) Preparation of the seed liquid of the white rot fungus: Inoculate the white rot bacteria of the white rot fungus on a newly prepared PDA plate with a diameter of 9 cm, activate the mycelia for 6 days to cover the plate, and inoculate one plate of bacteria The silk was inoculated into a shaker flask equipped with 400 mL of PDDA liquid medium, and cultured on a shaker at 29° C. for 88 hours to obtain a seed liquid of R. albicans.

[0025] (2) Inoculation and cultivation of the samara shell of Eucommia ulmoides: Soak the samara shell of Eucommia ulmoides in water for 19 hours and make the water content of the samara 69%, inoculate the seed liquid of eucommia samara according to 1.17% of the mass of the samara shell of Eucommia ulmoides, and The inoculated fruit shells are piled up for fermentation, and the ambient temperature is kept at 28°C and the humidity is 95% to ferment for 12 days. During the fermentation period, the fungus albicans occurs, and the shell material...

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Abstract

The invention discloses a eucommia ulmoides key fruit hull treating method beneficial to extraction of gutta-percha. The eucommia ulmoides key fruit hull treating method comprises the steps: (1), preparing an irpex lacteus seed solution; (2), inoculating and culturing a eucommia ulmoides key fruit hull; and (3), treating after fermenting. The dry weight of the treated eucommia ulmoides key fruit hull is reduced by 35-42 percent due to effective degradation of the irpex lacteus, the gutta-percha in the fruit hull can reach 50-60 percent, the efficiency and rate of extracting the gutta-percha by using organic solvents such as petroleum ether are greatly increased, and the glue quality is remarkably improved. The treatment effect of the eucommia ulmoides key fruit hull treating method is superior to an existing enzymic method and a distiller's yeast and yeast fermentation method; the eucommia ulmoides key fruit hull treating method has no damage to environment; the environment benefit of the eucommia ulmoides key fruit hull treating method is superior to that of an alkali treatment method; the eucommia ulmoides key fruit hull treating method is stronger in actual application value.

Description

technical field [0001] The invention relates to a method for processing eucommia samara shells, in particular to a method for enhancing the extraction of eucommia gum by treating the eucommia samurai shells with the eucommia alba. Background technique [0002] Eucommia gum is a new functional material. Eucommia gum and natural rubber produced in Hevea trilobata are isomers. Eucommia gum is trans-polyisoprene, and natural rubber is cis-polyisoprene. After vulcanization, Eucommia gum can be in rubber state or in different plastic states. There are many Eucommia gum products on the market, and its market application prospect is very broad. [0003] Eucommia gum mainly exists in the bark, leaves and fruits of Eucommia ulmoides, among which Eucommia samara has a gum content as high as 15%-30% and can be harvested every year, so it has become an ideal raw material for extracting Eucommia gum. In order to obtain eucommia gum with high purity, it is generally extracted with non-pol...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J3/00C08L7/00
Inventor 刘祝祥陈义光李克纲陈功锡黄诚张永康
Owner JISHOU UNIVERSITY
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