Antifogging coating, preparation method of antifogging coating and antifogging glass
An anti-fog coating and anti-fog layer technology, applied in the field of nanomaterials, can solve the problems of self-cleaning, poor anti-fog effect and durability, and achieve obvious anti-fog effect, wide application range, improved wear resistance and firm bonding degree of effect
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[0035] The invention provides a method for preparing the anti-fog coating. According to the difference in the number of layers of the cross-linked layer and the anti-fog layer, the preparation method is as follows:
[0036] When the anti-fog coating is composed of one layer of cross-linked layer and one layer of anti-fog layer, the preparation method of the anti-fog coating comprises the following steps: plate the cross-linked layer on the surface hydroxylated substrate, and carry out curing treatment ; Coating an anti-fog layer on the side of the cross-linked layer away from the substrate for curing.
[0037] When the anti-fog coating includes two or more cross-linked layers and two or more anti-fog layers, the preparation method of the anti-fog coating includes the following steps, step (1): plating the second layer on the surface hydroxylated substrate A cross-linked layer is subjected to curing treatment; the first anti-fog layer is coated on the side of the first cross-li...
Embodiment 1
[0045] This embodiment discloses an anti-fog coating composed of one layer of cross-linked layer and one layer of anti-fog layer. The preparation steps of anti-fog glass coated with the anti-fog coating are as follows:
[0046] (1) Hydroxylation of glass substrates: ultrasonically clean the clean glass substrates in deionized water, acetone, and deionized water for 5 minutes, 10 minutes, and 5 minutes, and rinse with a large amount of deionized water for several times; then place them in 30% H 2 o 2 with 98% concentrated H 2 SO 4 (1 / 3) was ultrasonically activated in the mixed solution for 30 minutes, washed with a large amount of deionized water until neutral; again ultrasonically cleaned in deionized water, acetone, and deionized water for 10 minutes, 5 minutes, and 5 minutes. The glass substrate was taken out, dried by nitrogen gas, and stored in vacuum at room temperature.
[0047] (2) Graft cross-linked layer: Dissolve styrene-maleic anhydride copolymer in a mixed solu...
Embodiment 2
[0051] This embodiment discloses an anti-fog coating consisting of two cross-linked layers and two anti-fog layers, the cross-linked layers and anti-fog layers are arranged alternately, and the anti-fog glass coated with the anti-fog coating The preparation steps are as follows:
[0052] (1) Hydroxylation of glass substrates: ultrasonically clean the clean glass substrates in deionized water, acetone, and deionized water for 5 minutes, 10 minutes, and 5 minutes, and rinse with a large amount of deionized water for several times; then place them in 30% H 2 o 2 with 98% concentrated H 2 SO 4 (1 / 3) was ultrasonically activated in the mixed solution for 30 minutes, washed with a large amount of deionized water until neutral; again ultrasonically cleaned in deionized water, acetone, and deionized water for 10 minutes, 5 minutes, and 5 minutes. The glass substrate was taken out, dried by nitrogen gas, and stored in vacuum at room temperature.
[0053] (2) Grafting the first cros...
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