Polybutylene terephthalate/glass fiber composite material and preparation method thereof
A technology of polybutylene terephthalate and glass fiber, which is applied in the field of polybutylene terephthalate/glass fiber composite material and its preparation, can solve the toughness of polybutylene terephthalate , processing performance and poor appearance quality, etc., to achieve good processing performance, solve the effect of enhancing the color and notched impact strength
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Embodiment 1~6
[0033] The preparation of embodiment 1~6 intermediate A and intermediate B
[0034] Intermediate A weighs various raw materials according to the raw material ratio in Table 1, and intermediate B weighs various raw materials according to the raw material ratio in Table 1.
[0035] Among them, PBT resin (molecular weight: 25000) was dried at 120°C for 5 hours before use, and various raw materials were added to a high-speed mixer and mixed at high speed for 3 minutes, and then discharged at a low speed. The mixed material is extruded and granulated to obtain intermediate A and intermediate B. Extrusion granulation conditions are: host screw speed 350r / min, feeding speed 30r / min, heating temperature range: 1 stage / 220°C, 2 stages / 230°C, 3 stages / 240°C, 4 stages / 250°C, 5 stages / 260°C, 6 stages / 250°C, 7 stages / 240°C, 8 stages / 230°C, 9 stages / 230°C, head temperature: 240°C.
Embodiment 7~9
[0040] The preparation of embodiment 7~9 polybutylene terephthalate / glass fiber composite material
[0041] The compositions of Examples 7-9 are shown in Table 2. Intermediate A and Intermediate B were uniformly mixed at a weight percentage of 1:1 to obtain a polybutylene terephthalate / glass fiber composite material.
[0042] Table 2 Composition and preparation of polybutylene terephthalate / glass fiber composites
[0043] product
Embodiment 10
[0044] Embodiment 10 performance comparison
[0045] The tensile strength and elongation at break of the products obtained in Comparative Examples 1 to 3 and the products obtained in Examples 7 to 9 were tested according to the national standard GB / T1040.2-2006; the flexural strength and flexural modulus were tested according to the national standard GB / T9341- Tested in 2000; Izod notched impact strength was tested in accordance with national standard GB / T1843-2008; melt flow rate was tested in accordance with national standard GB / T3682-2000. The performance comparison data of the products are shown in Table 3.
[0046] Table 3 Properties of polybutylene terephthalate / glass fiber composites
[0047]
[0048] As can be seen from table 1 and table 2, the product of embodiment 7 is identical with the glass fiber content of comparative example 2, and the product of embodiment 8 is identical with the glass fiber content of comparative example 3, as can be seen from table 3, by ...
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