Natural plant preservative taking rape seed cakes and folium ginkgo as raw materials as well as preparation method and application thereof
A technology of natural plants and rapeseed cakes, applied in the field of phytochemistry, can solve problems such as adverse effects on the natural ecological environment, chemical preservatives, threats to human health, etc., and achieve the effects of low cost, extended shelf life, and low price
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Embodiment 1
[0012] Dry the rapeseed cake and ginkgo leaves after black rapeseed oil extraction at 40-50°C for 2 days, take 700g of rapeseed cake and 300g of ginkgo leaves, mix well, grind them into powder, pass through a 40-mesh sieve, Have to mix the powder and set aside. At room temperature, use ethanol with a pH value of 1.0 and a concentration of 70% as the extraction solvent, put the mixed powder and the extraction solvent into the extraction container at a mass ratio of 1:12; ultrasonicate in an ultrasonic instrument at 600W and 40°C for 60 minutes, and then Use 600W microwave power to irradiate for 60s, filter and retain the filtrate; extract the filter residue once more in the same way, and combine the filtrate after the end. Concentrate in vacuum at 0-50°C to obtain solid powder; the solid powder is dried and crushed to 150 mesh to obtain rapeseed cake and ginkgo leaf extract, which are natural plant preservatives.
Embodiment 2
[0014] Dry the rapeseed cake and ginkgo leaves after black rapeseed oil extraction at 40-50°C for 2 days, take 750g of rapeseed cake and 250g of ginkgo leaves, mix well, grind them into powder, pass through a 40-mesh sieve, Have to mix the powder and set aside. At room temperature, use ethanol with a pH value of 1.5 and a concentration of 65% as the extraction solvent, put the mixed powder and the extraction solvent into the extraction container at a mass ratio of 1:10; ultrasonicate for 40 minutes at 500W and 45°C in an ultrasonic instrument, and then use Irradiate under 500W microwave power for 40s, filter and retain the filtrate; extract the filter residue once more according to the same method, and combine the filtrate after the end. Concentrate in vacuum at 0-50°C to obtain solid powder; the solid powder is dried and crushed to 150 mesh to obtain rapeseed cake and ginkgo leaf extract, which are natural plant preservatives.
Embodiment 3
[0016] Dry the rapeseed cake and ginkgo leaves after black rapeseed oil extraction at 40-50°C for 3 days, take 800g of rapeseed cake and 200g of ginkgo leaves, mix well, grind them into powder, pass through a 40-mesh sieve, Have to mix the powder and set aside. At room temperature, use ethanol with a pH value of 2.0 and a concentration of 75% as the extraction solvent, put the mixed powder and the extraction solvent into the extraction container at a mass ratio of 1:15; ultrasonicate for 30 minutes at 400W and 50°C in an ultrasonic instrument, and then use Irradiate under 400W microwave power for 30s, filter and retain the filtrate; extract the filter residue twice by weight according to the same method, and combine the filtrate after the end. Concentrate in vacuum at 0-50°C to obtain solid powder; the solid powder is dried and crushed to 150 mesh to obtain rapeseed cake and ginkgo leaf extract, which are natural plant preservatives.
[0017] Second, the antibacterial effect ...
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